N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate

In the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twi...

Full description

Bibliographic Details
Main Authors: Xue-Song Lin, Ya-Li Sang
Format: Article
Language:English
Published: International Union of Crystallography 2009-07-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809022983
_version_ 1819280117167292416
author Xue-Song Lin
Ya-Li Sang
author_facet Xue-Song Lin
Ya-Li Sang
author_sort Xue-Song Lin
collection DOAJ
description In the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds, forming layers parallel to the ac plane.
first_indexed 2024-12-24T00:38:42Z
format Article
id doaj.art-9f7c32420c414eb8ac6d27b20522d826
institution Directory Open Access Journal
issn 1600-5368
language English
last_indexed 2024-12-24T00:38:42Z
publishDate 2009-07-01
publisher International Union of Crystallography
record_format Article
series Acta Crystallographica Section E
spelling doaj.art-9f7c32420c414eb8ac6d27b20522d8262022-12-21T17:24:01ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-07-01657o1650o165010.1107/S1600536809022983N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvateXue-Song LinYa-Li SangIn the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds, forming layers parallel to the ac plane.http://scripts.iucr.org/cgi-bin/paper?S1600536809022983
spellingShingle Xue-Song Lin
Ya-Li Sang
N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
Acta Crystallographica Section E
title N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
title_full N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
title_fullStr N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
title_full_unstemmed N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
title_short N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
title_sort n amp 8242 5 bromo 2 methoxybenzylidene 4 hydroxybenzohydrazide methanol solvate
url http://scripts.iucr.org/cgi-bin/paper?S1600536809022983
work_keys_str_mv AT xuesonglin namp82425bromo2methoxybenzylidene4hydroxybenzohydrazidemethanolsolvate
AT yalisang namp82425bromo2methoxybenzylidene4hydroxybenzohydrazidemethanolsolvate