N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate
In the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twi...
Main Authors: | , |
---|---|
Format: | Article |
Language: | English |
Published: |
International Union of Crystallography
2009-07-01
|
Series: | Acta Crystallographica Section E |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809022983 |
_version_ | 1819280117167292416 |
---|---|
author | Xue-Song Lin Ya-Li Sang |
author_facet | Xue-Song Lin Ya-Li Sang |
author_sort | Xue-Song Lin |
collection | DOAJ |
description | In the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds, forming layers parallel to the ac plane. |
first_indexed | 2024-12-24T00:38:42Z |
format | Article |
id | doaj.art-9f7c32420c414eb8ac6d27b20522d826 |
institution | Directory Open Access Journal |
issn | 1600-5368 |
language | English |
last_indexed | 2024-12-24T00:38:42Z |
publishDate | 2009-07-01 |
publisher | International Union of Crystallography |
record_format | Article |
series | Acta Crystallographica Section E |
spelling | doaj.art-9f7c32420c414eb8ac6d27b20522d8262022-12-21T17:24:01ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-07-01657o1650o165010.1107/S1600536809022983N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvateXue-Song LinYa-Li SangIn the title hydrazone compound, C15H13BrN2O3·CH3OH, the methanol solvate is linked to the benzohydrazide molecule through O—H...N and O—H...O hydrogen bonds. The benzohydrazide molecule adopts an E configuration about the C=N double bond. The molecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds, forming layers parallel to the ac plane.http://scripts.iucr.org/cgi-bin/paper?S1600536809022983 |
spellingShingle | Xue-Song Lin Ya-Li Sang N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate Acta Crystallographica Section E |
title | N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate |
title_full | N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate |
title_fullStr | N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate |
title_full_unstemmed | N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate |
title_short | N′-(5-Bromo-2-methoxybenzylidene)-4-hydroxybenzohydrazide methanol solvate |
title_sort | n amp 8242 5 bromo 2 methoxybenzylidene 4 hydroxybenzohydrazide methanol solvate |
url | http://scripts.iucr.org/cgi-bin/paper?S1600536809022983 |
work_keys_str_mv | AT xuesonglin namp82425bromo2methoxybenzylidene4hydroxybenzohydrazidemethanolsolvate AT yalisang namp82425bromo2methoxybenzylidene4hydroxybenzohydrazidemethanolsolvate |