Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method
Novel Preparation of Co(II), Ni(II), Cu(II), and Zn(II) metal complexes was synthesized by the regular reflux method, and the nano-particles were prepared by using the thermal decomposition method. The synthesized ligand of 2,4-dichloro-6-((2-phenylhydrazono)methyl)phenol and metal complexes were co...
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| Format: | Article |
| Language: | English |
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Elsevier
2023-02-01
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| Series: | Applied Surface Science Advances |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S2666523922001477 |
| _version_ | 1797895560864202752 |
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| author | Usan Pathinathan Saleth Prabhakar |
| author_facet | Usan Pathinathan Saleth Prabhakar |
| author_sort | Usan Pathinathan Saleth Prabhakar |
| collection | DOAJ |
| description | Novel Preparation of Co(II), Ni(II), Cu(II), and Zn(II) metal complexes was synthesized by the regular reflux method, and the nano-particles were prepared by using the thermal decomposition method. The synthesized ligand of 2,4-dichloro-6-((2-phenylhydrazono)methyl)phenol and metal complexes were confirmed by spectral instruments like FTIR, UV, NMR, and Mass spectroscopy. By using the TGA spectrum the stability of the metal complexes was characterized. The morphology of the metal oxide was done by SEM analysis. The antimicrobial activity was carried out with free ligand and metal complexes. |
| first_indexed | 2024-04-10T07:27:46Z |
| format | Article |
| id | doaj.art-a01f0780f92545918be38825477b9c77 |
| institution | Directory Open Access Journal |
| issn | 2666-5239 |
| language | English |
| last_indexed | 2024-04-10T07:27:46Z |
| publishDate | 2023-02-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Applied Surface Science Advances |
| spelling | doaj.art-a01f0780f92545918be38825477b9c772023-02-24T04:31:44ZengElsevierApplied Surface Science Advances2666-52392023-02-0113100357Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition methodUsan Pathinathan Saleth Prabhakar0Correspondence Author.; Department of Chemistry, St. Joseph University, Dimapur 797 115, Nagaland, IndiaNovel Preparation of Co(II), Ni(II), Cu(II), and Zn(II) metal complexes was synthesized by the regular reflux method, and the nano-particles were prepared by using the thermal decomposition method. The synthesized ligand of 2,4-dichloro-6-((2-phenylhydrazono)methyl)phenol and metal complexes were confirmed by spectral instruments like FTIR, UV, NMR, and Mass spectroscopy. By using the TGA spectrum the stability of the metal complexes was characterized. The morphology of the metal oxide was done by SEM analysis. The antimicrobial activity was carried out with free ligand and metal complexes.http://www.sciencedirect.com/science/article/pii/S2666523922001477Schiff baseMetal oxideNmrTgaSemBiological Studies |
| spellingShingle | Usan Pathinathan Saleth Prabhakar Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method Applied Surface Science Advances Schiff base Metal oxide Nmr Tga Sem Biological Studies |
| title | Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| title_full | Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| title_fullStr | Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| title_full_unstemmed | Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| title_short | Synthesis, structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| title_sort | synthesis structural elucidation of metal nanoparticles prepared from metal complexes via thermal decomposition method |
| topic | Schiff base Metal oxide Nmr Tga Sem Biological Studies |
| url | http://www.sciencedirect.com/science/article/pii/S2666523922001477 |
| work_keys_str_mv | AT usanpathinathansalethprabhakar synthesisstructuralelucidationofmetalnanoparticlespreparedfrommetalcomplexesviathermaldecompositionmethod |