SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE
At present, chemistry teachers are searching new models that allow integrative laboratory experiences, converging interdisciplinary knowledge of the Chemistry field. With this framework of ideas, this work describes the synthesis and characterization of the (2E,6E)-2,6-bis(4-methoxybenzylidene)cyclo...
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| Format: | Article |
| Language: | Spanish |
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Executive Business School
2015-03-01
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| Series: | Avances en Ciencias e Ingeniería |
| Subjects: | |
| Online Access: | http://www.exeedu.com/publishing.cl/inicio.php?lnk=ctnd&id=328 |
| _version_ | 1818989040132685824 |
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| author | Perla E. Hernández-González Nancy Romero-Ceronio Cuauhtémoc Alvarado-Sánchez Abraham Gómez-Rivera Carlos E. Lobato-García Luis J. Romero-Morán |
| author_facet | Perla E. Hernández-González Nancy Romero-Ceronio Cuauhtémoc Alvarado-Sánchez Abraham Gómez-Rivera Carlos E. Lobato-García Luis J. Romero-Morán |
| author_sort | Perla E. Hernández-González |
| collection | DOAJ |
| description | At present, chemistry teachers are searching new models that allow integrative laboratory experiences, converging interdisciplinary knowledge of the Chemistry field. With this framework of ideas, this work describes the synthesis and characterization of the (2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone compound as axis of knowledge in order to encourage the students to develop their cognitive skills, such as critical thinking and problem solving, and also interpretation and analysis of results. The compound was synthesized by a Claisen-Schmidt condensation reaction, involving an aromatic aldehyde and cyclohexanone. The compound was characterized spectroscopically by NMR, IR and UV-Vis. Melting point and solubility tests were also performed. The chemical structure was confirmed by single crystal X-Ray diffraction. In conclusion, this laboratory experience allows students to get involved with the techniques and procedures commonly used in the organic chemistry laboratory to the synthesis and characterization of organic compounds. |
| first_indexed | 2024-12-20T19:32:09Z |
| format | Article |
| id | doaj.art-a061d52c44204501b88c2a06a825362e |
| institution | Directory Open Access Journal |
| issn | 0718-8706 0718-8706 |
| language | Spanish |
| last_indexed | 2024-12-20T19:32:09Z |
| publishDate | 2015-03-01 |
| publisher | Executive Business School |
| record_format | Article |
| series | Avances en Ciencias e Ingeniería |
| spelling | doaj.art-a061d52c44204501b88c2a06a825362e2022-12-21T19:28:46ZspaExecutive Business SchoolAvances en Ciencias e Ingeniería0718-87060718-87062015-03-01616372SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCEPerla E. Hernández-González0Nancy Romero-Ceronio1Cuauhtémoc Alvarado-Sánchez2Abraham Gómez-Rivera3Carlos E. Lobato-García4Luis J. Romero-Morán5Universidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoUniversidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoUniversidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoUniversidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoUniversidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoUniversidad Juárez Autónoma de Tabasco, División Académica de Ciencias Básicas, Carretera Cunduacán-Jalpa de Méndez Km 1, Cunduacán, Tabasco 86690 - MéxicoAt present, chemistry teachers are searching new models that allow integrative laboratory experiences, converging interdisciplinary knowledge of the Chemistry field. With this framework of ideas, this work describes the synthesis and characterization of the (2E,6E)-2,6-bis(4-methoxybenzylidene)cyclohexanone compound as axis of knowledge in order to encourage the students to develop their cognitive skills, such as critical thinking and problem solving, and also interpretation and analysis of results. The compound was synthesized by a Claisen-Schmidt condensation reaction, involving an aromatic aldehyde and cyclohexanone. The compound was characterized spectroscopically by NMR, IR and UV-Vis. Melting point and solubility tests were also performed. The chemical structure was confirmed by single crystal X-Ray diffraction. In conclusion, this laboratory experience allows students to get involved with the techniques and procedures commonly used in the organic chemistry laboratory to the synthesis and characterization of organic compounds.http://www.exeedu.com/publishing.cl/inicio.php?lnk=ctnd&id=328chalconescyclohexanonesynthesischaracterization |
| spellingShingle | Perla E. Hernández-González Nancy Romero-Ceronio Cuauhtémoc Alvarado-Sánchez Abraham Gómez-Rivera Carlos E. Lobato-García Luis J. Romero-Morán SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE Avances en Ciencias e Ingeniería chalcones cyclohexanone synthesis characterization |
| title | SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE |
| title_full | SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE |
| title_fullStr | SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE |
| title_full_unstemmed | SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE |
| title_short | SYNTHESIS AND CHARACTERIZATION OF A DERIVATIVE CYCLOHEXANONE CHALCONE-TYPE, AS AN INTEGRAL LABORATORY EXPERIENCE |
| title_sort | synthesis and characterization of a derivative cyclohexanone chalcone type as an integral laboratory experience |
| topic | chalcones cyclohexanone synthesis characterization |
| url | http://www.exeedu.com/publishing.cl/inicio.php?lnk=ctnd&id=328 |
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