Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)

用微波消解法处理样品,电感耦合等离子体质谱(ICP-MS)测定了11种卷烟烟草中的6种重金属元素.研究了微波消解和ICP-MS的测定条件.方法的检出限均小于1 μg/L,各元素测定的RSD(n=6)在0.29 %~3.55%,样品加标回收率为90.6%~104.9%.方法简便、快速、准确,适合用于测定烟草中的微量重金属元素,...

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Main Authors: HUANGXu(黄旭), XUZi-gang(徐子刚)
Format: Article
Language:zho
Published: Zhejiang University Press 2007-11-01
Series:Zhejiang Daxue xuebao. Lixue ban
Subjects:
Online Access:https://doi.org/zjup/1008-9497.2007.34.6.658-660
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author HUANGXu(黄旭)
XUZi-gang(徐子刚)
author_facet HUANGXu(黄旭)
XUZi-gang(徐子刚)
author_sort HUANGXu(黄旭)
collection DOAJ
description 用微波消解法处理样品,电感耦合等离子体质谱(ICP-MS)测定了11种卷烟烟草中的6种重金属元素.研究了微波消解和ICP-MS的测定条件.方法的检出限均小于1 μg/L,各元素测定的RSD(n=6)在0.29 %~3.55%,样品加标回收率为90.6%~104.9%.方法简便、快速、准确,适合用于测定烟草中的微量重金属元素,
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spelling doaj.art-a0f3deb031af4f78a4363f7b3a2fdfa52024-03-29T01:58:25ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972007-11-01346658660zjup/1008-9497.2007.34.6.658-660Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)HUANGXu(黄旭)0XUZi-gang(徐子刚)1Department of Chemistry, Zhejiang University, Hangzhou 310027, China(浙江大学化学系,浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, China(浙江大学化学系,浙江 杭州 310027)用微波消解法处理样品,电感耦合等离子体质谱(ICP-MS)测定了11种卷烟烟草中的6种重金属元素.研究了微波消解和ICP-MS的测定条件.方法的检出限均小于1 μg/L,各元素测定的RSD(n=6)在0.29 %~3.55%,样品加标回收率为90.6%~104.9%.方法简便、快速、准确,适合用于测定烟草中的微量重金属元素,https://doi.org/zjup/1008-9497.2007.34.6.658-660电感耦合等离子体质谱烟草重金属元素微波消解
spellingShingle HUANGXu(黄旭)
XUZi-gang(徐子刚)
Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
Zhejiang Daxue xuebao. Lixue ban
电感耦合等离子体质谱
烟草
重金属元素
微波消解
title Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
title_full Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
title_fullStr Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
title_full_unstemmed Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
title_short Determination of the heavy metal elements in tobacco by ICP-MS with microwave digestion(微波消解-电感耦合等离子体质谱法测定烟草中的重金属元素)
title_sort determination of the heavy metal elements in tobacco by icp ms with microwave digestion 微波消解 电感耦合等离子体质谱法测定烟草中的重金属元素
topic 电感耦合等离子体质谱
烟草
重金属元素
微波消解
url https://doi.org/zjup/1008-9497.2007.34.6.658-660
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