Identification and quantitation of lipid-bound short-chain diols

Procedures are described for the hydrolysis of neutral lipid fractions containing long-chain esters and alk-1-enyl ethers of short-chain diols, and for the identification and quantitation of the constituent diols as long-chain cyclic acetals using gas–liquid chromatography in combination with mass s...

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Bibliographic Details
Main Authors: E. Schupp, W.J. Baumann
Format: Article
Language:English
Published: Elsevier 1973-01-01
Series:Journal of Lipid Research
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0022227520393378
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author E. Schupp
W.J. Baumann
author_facet E. Schupp
W.J. Baumann
author_sort E. Schupp
collection DOAJ
description Procedures are described for the hydrolysis of neutral lipid fractions containing long-chain esters and alk-1-enyl ethers of short-chain diols, and for the identification and quantitation of the constituent diols as long-chain cyclic acetals using gas–liquid chromatography in combination with mass spectrometry.
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spelling doaj.art-a1412320527b4c84b2c40bd5047d77de2022-12-21T17:17:11ZengElsevierJournal of Lipid Research0022-22751973-01-01141121124Identification and quantitation of lipid-bound short-chain diolsE. Schupp0W.J. Baumann1University of Minnesota, The Hormel Institute, Austin, Minnesota 55912University of Minnesota, The Hormel Institute, Austin, Minnesota 55912Procedures are described for the hydrolysis of neutral lipid fractions containing long-chain esters and alk-1-enyl ethers of short-chain diols, and for the identification and quantitation of the constituent diols as long-chain cyclic acetals using gas–liquid chromatography in combination with mass spectrometry.http://www.sciencedirect.com/science/article/pii/S0022227520393378diol lipidsdiol estersdiol alk-1-enyl etherscyclic diol acetalsbarium hydroxideboron trifluoride
spellingShingle E. Schupp
W.J. Baumann
Identification and quantitation of lipid-bound short-chain diols
Journal of Lipid Research
diol lipids
diol esters
diol alk-1-enyl ethers
cyclic diol acetals
barium hydroxide
boron trifluoride
title Identification and quantitation of lipid-bound short-chain diols
title_full Identification and quantitation of lipid-bound short-chain diols
title_fullStr Identification and quantitation of lipid-bound short-chain diols
title_full_unstemmed Identification and quantitation of lipid-bound short-chain diols
title_short Identification and quantitation of lipid-bound short-chain diols
title_sort identification and quantitation of lipid bound short chain diols
topic diol lipids
diol esters
diol alk-1-enyl ethers
cyclic diol acetals
barium hydroxide
boron trifluoride
url http://www.sciencedirect.com/science/article/pii/S0022227520393378
work_keys_str_mv AT eschupp identificationandquantitationoflipidboundshortchaindiols
AT wjbaumann identificationandquantitationoflipidboundshortchaindiols