Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study
Phytic acid (IP6) has the ability to etch tooth structure due to its acidity and chelating properties. This study aimed to evaluate the micro-tensile bond strength (μTBS) of resin-based cement to enamel and dentin using manufacturer-provided etchants, phosphoric acid (PA) for enamel and a mixture of...
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MDPI AG
2021-12-01
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author | Mohannad Nassar Md. Sofiqul Islam Smriti Aryal A C Hatem Mostafa El-Damanhoury Salvatore Sauro Noriko Hiraishi |
author_facet | Mohannad Nassar Md. Sofiqul Islam Smriti Aryal A C Hatem Mostafa El-Damanhoury Salvatore Sauro Noriko Hiraishi |
author_sort | Mohannad Nassar |
collection | DOAJ |
description | Phytic acid (IP6) has the ability to etch tooth structure due to its acidity and chelating properties. This study aimed to evaluate the micro-tensile bond strength (μTBS) of resin-based cement to enamel and dentin using manufacturer-provided etchants, phosphoric acid (PA) for enamel and a mixture of 10% citric acid and 3% ferric chloride (CAF) for dentin and compare them to IP6. Enamel surfaces were etched for 30 s with either PA or IP6 (1%, 5% or 10%). Dentin surfaces were etched for 15 s with either CAF or 1% IP6. Pre-polymerized composite blocks were bonded to enamel and dentin surfaces. After 24 h, the specimens were sectioned into beams and subjected to μTBS testing. De-bonded specimens and smear layer removal were analyzed with a scanning electron microscope. Etching enamel with 1% and 5% IP6 resulted in μTBS values that are comparable to the control (PA) (<i>p</i> > 0.05), while 10% IP6 negatively affected the μTBS (<i>p</i> < 0.05). The μTBS to dentin etched with 1% IP6 was higher compared to the control (CAF) (<i>p</i> = 0.001). IP6 effectively removed enamel and dentin smear layer, and at specific concentrations, it may be a suitable alternative conditioner agent for bonding resin-based cement to enamel and dentin. |
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language | English |
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spelling | doaj.art-a202a9084aa94dc1b98ce96a85ed83192023-11-23T03:41:15ZengMDPI AGApplied Sciences2076-34172021-12-0111241197610.3390/app112411976Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro StudyMohannad Nassar0Md. Sofiqul Islam1Smriti Aryal A C2Hatem Mostafa El-Damanhoury3Salvatore Sauro4Noriko Hiraishi5Department of Preventive and Restorative Dentistry, College of Dental Medicine, University of Sharjah, Sharjah 27272, United Arab EmiratesOperative Dentistry, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah 30248, United Arab EmiratesDepartment of Oral and Craniofacial Health Sciences, College of Dental Medicine, University of Sharjah, Sharjah 27272, United Arab EmiratesDepartment of Preventive and Restorative Dentistry, College of Dental Medicine, University of Sharjah, Sharjah 27272, United Arab EmiratesDental Biomaterials and Minimally Invasive Dentistry, Departamento de Odontología, Facultad de Ciencias de la Salud, Universidad CEU-Cardenal Herrera, C/Del Pozo s/n, Alfara del Patriarca, 46115 Valencia, SpainCariology and Operative Dentistry, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, Tokyo 112-0000, JapanPhytic acid (IP6) has the ability to etch tooth structure due to its acidity and chelating properties. This study aimed to evaluate the micro-tensile bond strength (μTBS) of resin-based cement to enamel and dentin using manufacturer-provided etchants, phosphoric acid (PA) for enamel and a mixture of 10% citric acid and 3% ferric chloride (CAF) for dentin and compare them to IP6. Enamel surfaces were etched for 30 s with either PA or IP6 (1%, 5% or 10%). Dentin surfaces were etched for 15 s with either CAF or 1% IP6. Pre-polymerized composite blocks were bonded to enamel and dentin surfaces. After 24 h, the specimens were sectioned into beams and subjected to μTBS testing. De-bonded specimens and smear layer removal were analyzed with a scanning electron microscope. Etching enamel with 1% and 5% IP6 resulted in μTBS values that are comparable to the control (PA) (<i>p</i> > 0.05), while 10% IP6 negatively affected the μTBS (<i>p</i> < 0.05). The μTBS to dentin etched with 1% IP6 was higher compared to the control (CAF) (<i>p</i> = 0.001). IP6 effectively removed enamel and dentin smear layer, and at specific concentrations, it may be a suitable alternative conditioner agent for bonding resin-based cement to enamel and dentin.https://www.mdpi.com/2076-3417/11/24/11976phytic acidresin-based cementbond strengthdentinenamelsmear layer |
spellingShingle | Mohannad Nassar Md. Sofiqul Islam Smriti Aryal A C Hatem Mostafa El-Damanhoury Salvatore Sauro Noriko Hiraishi Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study Applied Sciences phytic acid resin-based cement bond strength dentin enamel smear layer |
title | Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study |
title_full | Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study |
title_fullStr | Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study |
title_full_unstemmed | Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study |
title_short | Resin-Based Cement Applied to Enamel and Dentin Pre-Treated with Phytic Acid: An In Vitro Study |
title_sort | resin based cement applied to enamel and dentin pre treated with phytic acid an in vitro study |
topic | phytic acid resin-based cement bond strength dentin enamel smear layer |
url | https://www.mdpi.com/2076-3417/11/24/11976 |
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