Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz
Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear 1D-NOE...
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| Format: | Article |
| Language: | deu |
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Swiss Chemical Society
1991-01-01
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| Series: | CHIMIA |
| Online Access: | https://chimia.ch/chimia/article/view/1987 |
| Summary: | Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear
1D-NOE spectroscopy, improved with respect to sensitivity and spectral quality, are demonstrated. These two methods allow structure elucidation by low sample amounts within reasonable measuring times.
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| ISSN: | 0009-4293 2673-2424 |