Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz
Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear 1D-NOE...
| Main Author: | |
|---|---|
| Format: | Article |
| Language: | deu |
| Published: |
Swiss Chemical Society
1991-01-01
|
| Series: | CHIMIA |
| Online Access: | https://chimia.ch/chimia/article/view/1987 |
| _version_ | 1818281887417761792 |
|---|---|
| author | Peter Bigler |
| author_facet | Peter Bigler |
| author_sort | Peter Bigler |
| collection | DOAJ |
| description |
Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear
1D-NOE spectroscopy, improved with respect to sensitivity and spectral quality, are demonstrated. These two methods allow structure elucidation by low sample amounts within reasonable measuring times.
|
| first_indexed | 2024-12-13T00:12:15Z |
| format | Article |
| id | doaj.art-a21ae874bdb043a0a5d10385e58ef31e |
| institution | Directory Open Access Journal |
| issn | 0009-4293 2673-2424 |
| language | deu |
| last_indexed | 2024-12-13T00:12:15Z |
| publishDate | 1991-01-01 |
| publisher | Swiss Chemical Society |
| record_format | Article |
| series | CHIMIA |
| spelling | doaj.art-a21ae874bdb043a0a5d10385e58ef31e2022-12-22T00:05:55ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241991-01-01451-2Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz Peter Bigler Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear 1D-NOE spectroscopy, improved with respect to sensitivity and spectral quality, are demonstrated. These two methods allow structure elucidation by low sample amounts within reasonable measuring times. https://chimia.ch/chimia/article/view/1987 |
| spellingShingle | Peter Bigler Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz CHIMIA |
| title | Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz |
| title_full | Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz |
| title_fullStr | Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz |
| title_full_unstemmed | Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz |
| title_short | Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz |
| title_sort | losung eines stereochemischen problems mit hilfe moderner methoden der hochauflosenden kernresonanz |
| url | https://chimia.ch/chimia/article/view/1987 |
| work_keys_str_mv | AT peterbigler losungeinesstereochemischenproblemsmithilfemodernermethodenderhochauflosendenkernresonanz |