9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione
The title compound, C23H24Cl2O3, was synthesized by reaction of 2,4-dichlorobenzaldehyde and 5,5-dimethylcyclohexane-1,3-dione in ethylene glycol. The central ring of the xanthene moiety is almost planar (with an r.m.s. deviation of 0.0268 Å from the least-squares plane) w...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2010-12-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810046702 |
| _version_ | 1818948452336271360 |
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| author | Hao Shi |
| author_facet | Hao Shi |
| author_sort | Hao Shi |
| collection | DOAJ |
| description | The title compound, C23H24Cl2O3, was synthesized by reaction of 2,4-dichlorobenzaldehyde and 5,5-dimethylcyclohexane-1,3-dione in ethylene glycol. The central ring of the xanthene moiety is almost planar (with an r.m.s. deviation of 0.0268 Å from the least-squares plane) while the two outer rings, in a cis arrangement, display envelope conformations. The ring of the 2,4-dichlorophenyl substituent is nearly perpendicular [85.89 (4)°] to the xanthene ring system. |
| first_indexed | 2024-12-20T08:47:01Z |
| format | Article |
| id | doaj.art-a2519c0d6cbf4e5c8ac2a798c46004d1 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T08:47:01Z |
| publishDate | 2010-12-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-a2519c0d6cbf4e5c8ac2a798c46004d12022-12-21T19:46:14ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-12-016612o3200o320010.1107/S16005368100467029-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dioneHao ShiThe title compound, C23H24Cl2O3, was synthesized by reaction of 2,4-dichlorobenzaldehyde and 5,5-dimethylcyclohexane-1,3-dione in ethylene glycol. The central ring of the xanthene moiety is almost planar (with an r.m.s. deviation of 0.0268 Å from the least-squares plane) while the two outer rings, in a cis arrangement, display envelope conformations. The ring of the 2,4-dichlorophenyl substituent is nearly perpendicular [85.89 (4)°] to the xanthene ring system.http://scripts.iucr.org/cgi-bin/paper?S1600536810046702 |
| spellingShingle | Hao Shi 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione Acta Crystallographica Section E |
| title | 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione |
| title_full | 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione |
| title_fullStr | 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione |
| title_full_unstemmed | 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione |
| title_short | 9-(2,4-Dichlorophenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione |
| title_sort | 9 2 4 dichlorophenyl 3 3 6 6 tetramethyl 3 4 5 6 tetrahydro 9h xanthene 1 8 2h 7h dione |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810046702 |
| work_keys_str_mv | AT haoshi 924dichlorophenyl3366tetramethyl3456tetrahydro9hxanthene182h7hdione |