In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification

The three-point bending behavior of a single Au nanowire deformed by an atomic force microscope was monitored by coherent X-ray diffraction using a sub-micrometer sized hard X-ray beam. Three-dimensional reciprocal-space maps were recorded before and after deformation by standard rocking curves and...

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Main Authors: Anton Davydok, Thomas W. Cornelius, Zhe Ren, Cedric Leclere, Gilbert Chahine, Tobias Schülli, Florian Lauraux, Gunther Richter, Olivier Thomas
Format: Article
Language:English
Published: MDPI AG 2018-11-01
Series:Quantum Beam Science
Subjects:
Online Access:https://www.mdpi.com/2412-382X/2/4/24
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author Anton Davydok
Thomas W. Cornelius
Zhe Ren
Cedric Leclere
Gilbert Chahine
Tobias Schülli
Florian Lauraux
Gunther Richter
Olivier Thomas
author_facet Anton Davydok
Thomas W. Cornelius
Zhe Ren
Cedric Leclere
Gilbert Chahine
Tobias Schülli
Florian Lauraux
Gunther Richter
Olivier Thomas
author_sort Anton Davydok
collection DOAJ
description The three-point bending behavior of a single Au nanowire deformed by an atomic force microscope was monitored by coherent X-ray diffraction using a sub-micrometer sized hard X-ray beam. Three-dimensional reciprocal-space maps were recorded before and after deformation by standard rocking curves and were measured by scanning the energy of the incident X-ray beam during deformation at different loading stages. The mechanical behavior of the nanowire was visualized in reciprocal space and a complex deformation mechanism is described. In addition to the expected bending of the nanowire, torsion was detected. Bending and torsion angles were quantified from the high-resolution diffraction data.
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spelling doaj.art-a2748da89e3044e98c09bac2ae5ade142022-12-21T21:41:19ZengMDPI AGQuantum Beam Science2412-382X2018-11-01242410.3390/qubs2040024qubs2040024In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and QuantificationAnton Davydok0Thomas W. Cornelius1Zhe Ren2Cedric Leclere3Gilbert Chahine4Tobias Schülli5Florian Lauraux6Gunther Richter7Olivier Thomas8CNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceCNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceCNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceCNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceID01/ESRF, 71 Avenue des Martyrs, CS40220, CEDEX 9, F-38043 Grenoble, FranceID01/ESRF, 71 Avenue des Martyrs, CS40220, CEDEX 9, F-38043 Grenoble, FranceCNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceMax Planck Institute for Intelligent Systems, Heisenbergstrasse 3, 70569 Stuttgart, GermanyCNRS, Aix Marseille University, University de Toulon, IM2NP Marseille, FranceThe three-point bending behavior of a single Au nanowire deformed by an atomic force microscope was monitored by coherent X-ray diffraction using a sub-micrometer sized hard X-ray beam. Three-dimensional reciprocal-space maps were recorded before and after deformation by standard rocking curves and were measured by scanning the energy of the incident X-ray beam during deformation at different loading stages. The mechanical behavior of the nanowire was visualized in reciprocal space and a complex deformation mechanism is described. In addition to the expected bending of the nanowire, torsion was detected. Bending and torsion angles were quantified from the high-resolution diffraction data.https://www.mdpi.com/2412-382X/2/4/24synchrotron X-ray diffractionnanostructuresnanomechanics
spellingShingle Anton Davydok
Thomas W. Cornelius
Zhe Ren
Cedric Leclere
Gilbert Chahine
Tobias Schülli
Florian Lauraux
Gunther Richter
Olivier Thomas
In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
Quantum Beam Science
synchrotron X-ray diffraction
nanostructures
nanomechanics
title In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
title_full In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
title_fullStr In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
title_full_unstemmed In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
title_short In Situ Coherent X-ray Diffraction during Three-Point Bending of a Au Nanowire: Visualization and Quantification
title_sort in situ coherent x ray diffraction during three point bending of a au nanowire visualization and quantification
topic synchrotron X-ray diffraction
nanostructures
nanomechanics
url https://www.mdpi.com/2412-382X/2/4/24
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