Meso-structure and fracture mechanism of mudstone at high temperature

The meso-structure mineral composition and fracture mechanism of uniaxial compressed mudstone samples at high temperature were analyzed by XRD and scanning electron microscopy. The effect of temperature on mudstone composition and fracture mechanism were studied from a meso-structural perspective, a...

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Bibliographic Details
Main Authors: Lianying Zhang, Xianbiao Mao, Ruixue Liu, Yan Li, Huiguang Yin
Format: Article
Language:English
Published: Elsevier 2014-07-01
Series:International Journal of Mining Science and Technology
Online Access:http://www.sciencedirect.com/science/article/pii/S2095268614000767
Description
Summary:The meso-structure mineral composition and fracture mechanism of uniaxial compressed mudstone samples at high temperature were analyzed by XRD and scanning electron microscopy. The effect of temperature on mudstone composition and fracture mechanism were studied from a meso-structural perspective, and the relationship between meso-structure and macro-mechanical characteristics at high temperature was revealed. The findings demonstrated that the fluctuation in diffraction intensity of kaolinite in the mudstone caused the fluctuation in its mechanical properties. The overall structure underwent a phase change around 600 °C, which led to the sudden change in the mechanical properties of mudstone samples. When the temperature reached 600 °C, the crystalline state worsened and kaolinite disappeared; however, some illite was produced, indicating that the chemical reaction of the structure and sudden drop of bearing capacity of the mudstone. Mudstone fracturing at high temperature involves mainly intergranular and transgranular fractures, which are typical in micro-brittle tensile failure. Considering the macro-fracture characteristics of mudstone, the results suggested that macro-fracture under external force corresponds to the meso-fracture. Keywords: Mudstone, Mineral composition, SEM, Meso-fracture, Macro-fracture
ISSN:2095-2686