Synthesis and structure of photodegradable 1-(4,5-dimethoxy-2,3-dinitrophenyl)-2-methylpropyl N-butylcarbamate

Synthesis and structure of photodegradable 1-(4,5-dimethoxy-2,3-dinitrophenyl)-2-methylpropyl N-butylcarbamate

The reaction of 1-(4,5-dimethoxy-2,3-dinitrophenyl)-2-methylpropan-1-ol and butylisocyanate using dibutyltin dilaurate as a catalyst afforded 1-(4,5-dimethoxy-2,3-dinitrophenyl)-2-methylpropyl N-butylcarbamate, C17H25N3O8, which released butylamine upon photoirradiation. Single crystals of the title...

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Bibliographic Details
Main Authors: Takafumi Honda, Michiko Ito, Kazuo Yamaguchi, Noriko Chikaraishi Kasuga, Hiroyasu Sato
Format: Article
Language:English
Published: International Union of Crystallography 2023-06-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
photolabile carbamate
2,3-dinitrobenzyl group
intermolecular hydrogen bonding
crystal structure
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989023004103

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