Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures

The wear resistance of TC4 titanium alloy was improved by plasma nitriding and the optimum nitriding temperature was investigated. TC4 titanium alloy was nitrided at 650, 700, 750, 800, 850℃ and 900℃ with LDM1-100 plasma nitriding equipment respectively,the temperature holding time is 10 h for each...

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Main Authors: YUAN Yun-gang, KANG Jia-jie, YUE Wen, FU Zhi-qiang, ZHU Li-na, SHE Ding-shun, WANG Cheng-biao
Format: Article
Language:zho
Published: Journal of Materials Engineering 2019-02-01
Series:Cailiao gongcheng
Subjects:
Online Access:http://html.rhhz.net/CHXB/html/2020-2-156.htm
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author YUAN Yun-gang
KANG Jia-jie
YUE Wen
FU Zhi-qiang
ZHU Li-na
SHE Ding-shun
WANG Cheng-biao
author_facet YUAN Yun-gang
KANG Jia-jie
YUE Wen
FU Zhi-qiang
ZHU Li-na
SHE Ding-shun
WANG Cheng-biao
author_sort YUAN Yun-gang
collection DOAJ
description The wear resistance of TC4 titanium alloy was improved by plasma nitriding and the optimum nitriding temperature was investigated. TC4 titanium alloy was nitrided at 650, 700, 750, 800, 850℃ and 900℃ with LDM1-100 plasma nitriding equipment respectively,the temperature holding time is 10 h for each nitriding treatment. The microstructure, surface morphology, surface roughness, phase structure and hardness of nitrided samples at different temperatures were characterized by optical microscope, scanning electron microscope, white light three-dimensional topography instrument and microhardness tester. The tribological properties of TC4 titanium alloy after plasma nitriding were tested by CETR UMT-3 multifunctional friction and wear tester. The results show that the surface microhardness and roughness of TC4 titanium alloy increase with the increase of temperature. After nitriding at 900℃, the surface microhardness of TC4 titanium alloy reaches 1318HV<sub>0.05</sub>, which is about 4 times as high as that of the substrate (360HV<sub>0.05</sub>). The increase of hardness is due to the formation of hard nitride phases (TiN and Ti<sub>2</sub>N phases) on the surface of nitrided sample and the nitride content increases with the increase of nitriding temperature. The load-carrying capacity of nitrided samples at 800℃ and 900℃ is significantly higher than that of nitriding samples at low temperatures (below 750℃). Compared with the original TC4 sample, the wear volume of the nitrided sample significantly reduces. When nitriding temperature is 850℃, the wear volume of the nitrided sample is 1.2% (1 N), 3.0% (3 N) and 62.2% (5 N) of that of the untreated sample, and the improvement of wear resistance of the sample is the most obvious.
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spelling doaj.art-a309f3bf870d484c81be05b8654610ce2023-01-02T18:50:38ZzhoJournal of Materials EngineeringCailiao gongcheng1001-43811001-43812019-02-0148215616220200221Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperaturesYUAN Yun-gang0KANG Jia-jie1YUE Wen2FU Zhi-qiang3ZHU Li-na4SHE Ding-shun5WANG Cheng-biao6School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;School of Engineering and Technology, China University of Geosciences(Beijing), Beijing 100083, China;Zhengzhou Institute, China University of Geosciences(Beijing), Zhengzhou 451283, China;The wear resistance of TC4 titanium alloy was improved by plasma nitriding and the optimum nitriding temperature was investigated. TC4 titanium alloy was nitrided at 650, 700, 750, 800, 850℃ and 900℃ with LDM1-100 plasma nitriding equipment respectively,the temperature holding time is 10 h for each nitriding treatment. The microstructure, surface morphology, surface roughness, phase structure and hardness of nitrided samples at different temperatures were characterized by optical microscope, scanning electron microscope, white light three-dimensional topography instrument and microhardness tester. The tribological properties of TC4 titanium alloy after plasma nitriding were tested by CETR UMT-3 multifunctional friction and wear tester. The results show that the surface microhardness and roughness of TC4 titanium alloy increase with the increase of temperature. After nitriding at 900℃, the surface microhardness of TC4 titanium alloy reaches 1318HV<sub>0.05</sub>, which is about 4 times as high as that of the substrate (360HV<sub>0.05</sub>). The increase of hardness is due to the formation of hard nitride phases (TiN and Ti<sub>2</sub>N phases) on the surface of nitrided sample and the nitride content increases with the increase of nitriding temperature. The load-carrying capacity of nitrided samples at 800℃ and 900℃ is significantly higher than that of nitriding samples at low temperatures (below 750℃). Compared with the original TC4 sample, the wear volume of the nitrided sample significantly reduces. When nitriding temperature is 850℃, the wear volume of the nitrided sample is 1.2% (1 N), 3.0% (3 N) and 62.2% (5 N) of that of the untreated sample, and the improvement of wear resistance of the sample is the most obvious.http://html.rhhz.net/CHXB/html/2020-2-156.htmtc4 titanium alloyplasma nitridingmicrostructuretribological propertywear resistance
spellingShingle YUAN Yun-gang
KANG Jia-jie
YUE Wen
FU Zhi-qiang
ZHU Li-na
SHE Ding-shun
WANG Cheng-biao
Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
Cailiao gongcheng
tc4 titanium alloy
plasma nitriding
microstructure
tribological property
wear resistance
title Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
title_full Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
title_fullStr Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
title_full_unstemmed Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
title_short Tribological properties of TC4 titanium alloy treated by plasma nitriding at different temperatures
title_sort tribological properties of tc4 titanium alloy treated by plasma nitriding at different temperatures
topic tc4 titanium alloy
plasma nitriding
microstructure
tribological property
wear resistance
url http://html.rhhz.net/CHXB/html/2020-2-156.htm
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AT fuzhiqiang tribologicalpropertiesoftc4titaniumalloytreatedbyplasmanitridingatdifferenttemperatures
AT zhulina tribologicalpropertiesoftc4titaniumalloytreatedbyplasmanitridingatdifferenttemperatures
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