Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen

In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon®) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon t...

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Bibliographic Details
Main Authors: Kevin Pels, Veljko Dragojlovic
Format: Article
Language:English
Published: Beilstein-Institut 2009-12-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
Online Access:https://doi.org/10.3762/bjoc.5.75
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author Kevin Pels
Veljko Dragojlovic
author_facet Kevin Pels
Veljko Dragojlovic
author_sort Kevin Pels
collection DOAJ
description In a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon®) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon the densities of the reactants and the procedure generates little or no waste while providing the reaction products in high yield and in high purity.
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spelling doaj.art-a3893c68dc2345a284e4a4e332e524e02022-12-21T22:47:23ZengBeilstein-InstitutBeilstein Journal of Organic Chemistry1860-53972009-12-01517510.3762/bjoc.5.751860-5397-5-75Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screenKevin Pels0Veljko Dragojlovic1Wilkes Honors College of Florida Atlantic University, 5353 Parkside Drive, Jupiter, FL 33458, USAWilkes Honors College of Florida Atlantic University, 5353 Parkside Drive, Jupiter, FL 33458, USAIn a solvent-free phase-vanishing reaction with PTFE (polytetrafluoroethylene, Teflon®) tape as the phase screen, a thermometer adapter is utilized to insert a PTFE-sealed tube into the vapor phase above the substrate. Besides avoiding use of solvents, the experimental design is not dependent upon the densities of the reactants and the procedure generates little or no waste while providing the reaction products in high yield and in high purity.https://doi.org/10.3762/bjoc.5.75brominationphase-vanishingPTFEsolvent-freestilbene
spellingShingle Kevin Pels
Veljko Dragojlovic
Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
Beilstein Journal of Organic Chemistry
bromination
phase-vanishing
PTFE
solvent-free
stilbene
title Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
title_full Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
title_fullStr Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
title_full_unstemmed Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
title_short Solvent-free phase-vanishing reactions with PTFE (Teflon®) as a phase screen
title_sort solvent free phase vanishing reactions with ptfe teflon r as a phase screen
topic bromination
phase-vanishing
PTFE
solvent-free
stilbene
url https://doi.org/10.3762/bjoc.5.75
work_keys_str_mv AT kevinpels solventfreephasevanishingreactionswithptfeteflonasaphasescreen
AT veljkodragojlovic solventfreephasevanishingreactionswithptfeteflonasaphasescreen