Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate
The title hydrated salt, 2C5H8N3+·C8H5O4−·NO3−·H2O, was obtained fortuitously from the reaction between 2,6-diaminopyridine, phthalic acid and Co(NO3)2·6H2O at 343 K. The asymmetric unit consists of two cry...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2010-03-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810004150 |
| _version_ | 1818791620271669248 |
|---|---|
| author | Mehrdad Pourayoubi Maryam Safaeimovahed Akbar Raissi Shabari |
| author_facet | Mehrdad Pourayoubi Maryam Safaeimovahed Akbar Raissi Shabari |
| author_sort | Mehrdad Pourayoubi |
| collection | DOAJ |
| description | The title hydrated salt, 2C5H8N3+·C8H5O4−·NO3−·H2O, was obtained fortuitously from the reaction between 2,6-diaminopyridine, phthalic acid and Co(NO3)2·6H2O at 343 K. The asymmetric unit consists of two crystallographically independent 2,6-diaminopyridinium cations, a hydrogen phthalate anion, a nitrate ion and a water molecule of crystallization which in the crystal structure are linked by intermolecular O—H...O and N—H...O hydrogen bonds into a three-dimensional network. In the hydrogen phthalate anion, there is a very strong intramolecular O—H...O hydrogen bond. |
| first_indexed | 2024-12-18T15:14:15Z |
| format | Article |
| id | doaj.art-a3e97d77c33749a8b2111a64ed13018c |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-18T15:14:15Z |
| publishDate | 2010-03-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-a3e97d77c33749a8b2111a64ed13018c2022-12-21T21:03:34ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-03-01663o551o55110.1107/S1600536810004150Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrateMehrdad PourayoubiMaryam SafaeimovahedAkbar Raissi ShabariThe title hydrated salt, 2C5H8N3+·C8H5O4−·NO3−·H2O, was obtained fortuitously from the reaction between 2,6-diaminopyridine, phthalic acid and Co(NO3)2·6H2O at 343 K. The asymmetric unit consists of two crystallographically independent 2,6-diaminopyridinium cations, a hydrogen phthalate anion, a nitrate ion and a water molecule of crystallization which in the crystal structure are linked by intermolecular O—H...O and N—H...O hydrogen bonds into a three-dimensional network. In the hydrogen phthalate anion, there is a very strong intramolecular O—H...O hydrogen bond.http://scripts.iucr.org/cgi-bin/paper?S1600536810004150 |
| spellingShingle | Mehrdad Pourayoubi Maryam Safaeimovahed Akbar Raissi Shabari Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate Acta Crystallographica Section E |
| title | Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate |
| title_full | Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate |
| title_fullStr | Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate |
| title_full_unstemmed | Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate |
| title_short | Bis(2,6-diaminopyridinium) hydrogen phthalate nitrate monohydrate |
| title_sort | bis 2 6 diaminopyridinium hydrogen phthalate nitrate monohydrate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810004150 |
| work_keys_str_mv | AT mehrdadpourayoubi bis26diaminopyridiniumhydrogenphthalatenitratemonohydrate AT maryamsafaeimovahed bis26diaminopyridiniumhydrogenphthalatenitratemonohydrate AT akbarraissishabari bis26diaminopyridiniumhydrogenphthalatenitratemonohydrate |