2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1<i>H</i>-[<i>d</i>]-1,3,2-benzodiazaborole
In this paper, a synthesis and characterization of a novel three coordinate 2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1<i>H</i>-[<i>d</i>]-1,3,2-benzodiazaborole from a cyclo-condensation reaction of <i>o</i>-phenylenediamine and 10-bromoanthracene-9-boronic acid is...
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| Format: | Article |
| Language: | English |
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MDPI AG
2023-01-01
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| Series: | Molbank |
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| Online Access: | https://www.mdpi.com/1422-8599/2023/1/M1569 |
| Summary: | In this paper, a synthesis and characterization of a novel three coordinate 2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1<i>H</i>-[<i>d</i>]-1,3,2-benzodiazaborole from a cyclo-condensation reaction of <i>o</i>-phenylenediamine and 10-bromoanthracene-9-boronic acid is described. The desired product was obtained in 0.343 g (92% yields) with its structure characterized by <sup>1</sup>H, <sup>11</sup>B, <sup>13</sup>C NMR, HRMS and FT-IR. |
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| ISSN: | 1422-8599 |