Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process

Soft magnetic Fe81.3Si4B10P4Cu0.7 powders have been fabricated by using spinning-water atomization process (SWAP) under the water pressure of 17.5 MPa and gas pressure of 2 MPa. To clarify the amorphous forming ability, thermal stability, and the corresponding soft magnetism, the as-SWAPed powders h...

Full description

Bibliographic Details
Main Authors: Jiawei LI, Zihao XU, Zhenhua DAN, Hui CHANG, Akihiro MAKINO
Format: Article
Language:English
Published: Kaunas University of Technology 2022-08-01
Series:Medžiagotyra
Subjects:
Online Access:https://matsc.ktu.lt/index.php/MatSc/article/view/30017
_version_ 1797773159966965760
author Jiawei LI
Zihao XU
Zhenhua DAN
Hui CHANG
Akihiro MAKINO
author_facet Jiawei LI
Zihao XU
Zhenhua DAN
Hui CHANG
Akihiro MAKINO
author_sort Jiawei LI
collection DOAJ
description Soft magnetic Fe81.3Si4B10P4Cu0.7 powders have been fabricated by using spinning-water atomization process (SWAP) under the water pressure of 17.5 MPa and gas pressure of 2 MPa. To clarify the amorphous forming ability, thermal stability, and the corresponding soft magnetism, the as-SWAPed powders have been sieved into 6 groups with different powder sizes from 0 – 150 μm. After the analysis of the amorphous and crystalline characteristics, the morphology, and soft magnetic properties of these 6 groups of as-SWAPed powders, it is concluded that the SWAPs with a high cooling rate of 105 K/s can improve the amorphous forming abilities of Fe81.3Si4B10P4Cu0.7 powders up to 53 μm, the saturated magnetic flux density as high as 170 – 173 emu/g and the thermal stabilities higher than 112.8 K. The characteristic parameters of as-SWAPed powders above mentioned are close to those of the counterpart rapid solidified ribbons. The surface oxide layers on as-SWAPed powders mainly consist of Fe2O3, and are 10 nm thick, much thicker than these counterpart ribbons, which might help to weaken the eddy effects accompanying with the slight decrease of the saturated magnetic flux density. Due to the higher cooling rates of SWAPs than gas atomization processes and the better spheroidization of powders for SWAPs than water atomization processes, it is key for NANOMET® family alloys to increase their amorphous forming abilities and better the soft magnetic performances.
first_indexed 2024-03-12T22:02:21Z
format Article
id doaj.art-a430f1efa8db444a87e8d6996c794d10
institution Directory Open Access Journal
issn 1392-1320
2029-7289
language English
last_indexed 2024-03-12T22:02:21Z
publishDate 2022-08-01
publisher Kaunas University of Technology
record_format Article
series Medžiagotyra
spelling doaj.art-a430f1efa8db444a87e8d6996c794d102023-07-25T04:41:47ZengKaunas University of TechnologyMedžiagotyra1392-13202029-72892022-08-0128331532110.5755/j02.ms.3001735271Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization ProcessJiawei LI0Zihao XU1Zhenhua DAN2https://orcid.org/0000-0002-3026-685XHui CHANG3Akihiro MAKINO4Nanjing Tech UniversityNanjing Tech UniversityNanjing Tech UniversityNanjing Tech UniversityTohoku UniversitySoft magnetic Fe81.3Si4B10P4Cu0.7 powders have been fabricated by using spinning-water atomization process (SWAP) under the water pressure of 17.5 MPa and gas pressure of 2 MPa. To clarify the amorphous forming ability, thermal stability, and the corresponding soft magnetism, the as-SWAPed powders have been sieved into 6 groups with different powder sizes from 0 – 150 μm. After the analysis of the amorphous and crystalline characteristics, the morphology, and soft magnetic properties of these 6 groups of as-SWAPed powders, it is concluded that the SWAPs with a high cooling rate of 105 K/s can improve the amorphous forming abilities of Fe81.3Si4B10P4Cu0.7 powders up to 53 μm, the saturated magnetic flux density as high as 170 – 173 emu/g and the thermal stabilities higher than 112.8 K. The characteristic parameters of as-SWAPed powders above mentioned are close to those of the counterpart rapid solidified ribbons. The surface oxide layers on as-SWAPed powders mainly consist of Fe2O3, and are 10 nm thick, much thicker than these counterpart ribbons, which might help to weaken the eddy effects accompanying with the slight decrease of the saturated magnetic flux density. Due to the higher cooling rates of SWAPs than gas atomization processes and the better spheroidization of powders for SWAPs than water atomization processes, it is key for NANOMET® family alloys to increase their amorphous forming abilities and better the soft magnetic performances.https://matsc.ktu.lt/index.php/MatSc/article/view/30017spinning-water atomization processfe81.3si4b10p4cu0.7 amorphous powdersamorphous forming abilitythermal stabilitysoft magnetic performance
spellingShingle Jiawei LI
Zihao XU
Zhenhua DAN
Hui CHANG
Akihiro MAKINO
Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
Medžiagotyra
spinning-water atomization process
fe81.3si4b10p4cu0.7 amorphous powders
amorphous forming ability
thermal stability
soft magnetic performance
title Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
title_full Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
title_fullStr Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
title_full_unstemmed Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
title_short Fabrication and Soft Magnetic Properties of Fe81.3Si4B10P4Cu0.7 Amorphous Powders by Using the Spinning-water Atomization Process
title_sort fabrication and soft magnetic properties of fe81 3si4b10p4cu0 7 amorphous powders by using the spinning water atomization process
topic spinning-water atomization process
fe81.3si4b10p4cu0.7 amorphous powders
amorphous forming ability
thermal stability
soft magnetic performance
url https://matsc.ktu.lt/index.php/MatSc/article/view/30017
work_keys_str_mv AT jiaweili fabricationandsoftmagneticpropertiesoffe813si4b10p4cu07amorphouspowdersbyusingthespinningwateratomizationprocess
AT zihaoxu fabricationandsoftmagneticpropertiesoffe813si4b10p4cu07amorphouspowdersbyusingthespinningwateratomizationprocess
AT zhenhuadan fabricationandsoftmagneticpropertiesoffe813si4b10p4cu07amorphouspowdersbyusingthespinningwateratomizationprocess
AT huichang fabricationandsoftmagneticpropertiesoffe813si4b10p4cu07amorphouspowdersbyusingthespinningwateratomizationprocess
AT akihiromakino fabricationandsoftmagneticpropertiesoffe813si4b10p4cu07amorphouspowdersbyusingthespinningwateratomizationprocess