Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology

Zinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The a...

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Main Authors: Mikrajuddin Abdullah, Kikuo Okuyama
Format: Article
Language:English
Published: ITB Journal Publisher 2004-11-01
Series:ITB Journal of Engineering Science
Subjects:
Online Access:http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37
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author Mikrajuddin Abdullah
Kikuo Okuyama
author_facet Mikrajuddin Abdullah
Kikuo Okuyama
author_sort Mikrajuddin Abdullah
collection DOAJ
description Zinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The absence of polymer led to the presence of several micrometer-sized flakes. In addition, the heating temperatures must be higher than 500˚C to completely decompose the organic material in final product. However, if zinc acetate was used as precursor, nanometer-sized ZnO having a high crystallinity can be obtained even when the polymer was absent. Interestingly, we also found that heating at low temperatures (e.g. 400˚C) resulted in ZnO nanorods with an elongation ratio of around 5. This method is rapid, economically efficient, and readily scalable for industrial applications.
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spelling doaj.art-a48e74fefde44c91a7c743f8cff55dad2022-12-21T23:57:27ZengITB Journal PublisherITB Journal of Engineering Science1978-30512004-11-01362141153Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the MorphologyMikrajuddin AbdullahKikuo OkuyamaZinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The absence of polymer led to the presence of several micrometer-sized flakes. In addition, the heating temperatures must be higher than 500˚C to completely decompose the organic material in final product. However, if zinc acetate was used as precursor, nanometer-sized ZnO having a high crystallinity can be obtained even when the polymer was absent. Interestingly, we also found that heating at low temperatures (e.g. 400˚C) resulted in ZnO nanorods with an elongation ratio of around 5. This method is rapid, economically efficient, and readily scalable for industrial applications.http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37Zinc oxide nanoparticleszinc oxide nanorodscrystallinityparticle size
spellingShingle Mikrajuddin Abdullah
Kikuo Okuyama
Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
ITB Journal of Engineering Science
Zinc oxide nanoparticles
zinc oxide nanorods
crystallinity
particle size
title Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
title_full Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
title_fullStr Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
title_full_unstemmed Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
title_short Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
title_sort zinc oxide nanoparticles prepared by a simple heating effect of polymer addition and polymer absence on the morphology
topic Zinc oxide nanoparticles
zinc oxide nanorods
crystallinity
particle size
url http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37
work_keys_str_mv AT mikrajuddinabdullah zincoxidenanoparticlespreparedbyasimpleheatingeffectofpolymeradditionandpolymerabsenceonthemorphology
AT kikuookuyama zincoxidenanoparticlespreparedbyasimpleheatingeffectofpolymeradditionandpolymerabsenceonthemorphology