Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology
Zinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The a...
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ITB Journal Publisher
2004-11-01
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Series: | ITB Journal of Engineering Science |
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Online Access: | http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37 |
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author | Mikrajuddin Abdullah Kikuo Okuyama |
author_facet | Mikrajuddin Abdullah Kikuo Okuyama |
author_sort | Mikrajuddin Abdullah |
collection | DOAJ |
description | Zinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The absence of polymer led to the presence of several micrometer-sized flakes. In addition, the heating temperatures must be higher than 500˚C to completely decompose the organic material in final product. However, if zinc acetate was used as precursor, nanometer-sized ZnO having a high crystallinity can be obtained even when the polymer was absent. Interestingly, we also found that heating at low temperatures (e.g. 400˚C) resulted in ZnO nanorods with an elongation ratio of around 5. This method is rapid, economically efficient, and readily scalable for industrial applications. |
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institution | Directory Open Access Journal |
issn | 1978-3051 |
language | English |
last_indexed | 2024-12-13T05:55:46Z |
publishDate | 2004-11-01 |
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spelling | doaj.art-a48e74fefde44c91a7c743f8cff55dad2022-12-21T23:57:27ZengITB Journal PublisherITB Journal of Engineering Science1978-30512004-11-01362141153Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the MorphologyMikrajuddin AbdullahKikuo OkuyamaZinc oxide (ZnO) nanoparticles were prepared by a simple heating of precursors in a furnace at temperatures of below 1000˚C in an air environment. If zinc nitrate was used as precursor, polymer (e.g., polyethylene glycol (PEG)) must be added into the precursor to produce ZnO in nanometer size. The absence of polymer led to the presence of several micrometer-sized flakes. In addition, the heating temperatures must be higher than 500˚C to completely decompose the organic material in final product. However, if zinc acetate was used as precursor, nanometer-sized ZnO having a high crystallinity can be obtained even when the polymer was absent. Interestingly, we also found that heating at low temperatures (e.g. 400˚C) resulted in ZnO nanorods with an elongation ratio of around 5. This method is rapid, economically efficient, and readily scalable for industrial applications.http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37Zinc oxide nanoparticleszinc oxide nanorodscrystallinityparticle size |
spellingShingle | Mikrajuddin Abdullah Kikuo Okuyama Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology ITB Journal of Engineering Science Zinc oxide nanoparticles zinc oxide nanorods crystallinity particle size |
title | Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology |
title_full | Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology |
title_fullStr | Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology |
title_full_unstemmed | Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology |
title_short | Zinc Oxide Nanoparticles Prepared By a Simple Heating: Effect of Polymer Addition and Polymer Absence on the Morphology |
title_sort | zinc oxide nanoparticles prepared by a simple heating effect of polymer addition and polymer absence on the morphology |
topic | Zinc oxide nanoparticles zinc oxide nanorods crystallinity particle size |
url | http://journal.itb.ac.id/download.php?file=B04009.pdf&id=75&up=37 |
work_keys_str_mv | AT mikrajuddinabdullah zincoxidenanoparticlespreparedbyasimpleheatingeffectofpolymeradditionandpolymerabsenceonthemorphology AT kikuookuyama zincoxidenanoparticlespreparedbyasimpleheatingeffectofpolymeradditionandpolymerabsenceonthemorphology |