Synthesis and Characterization of Thermally-Reduced Graphene
Thermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectrosc...
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Format: | Article |
Language: | English |
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Babol Noshirvani University of Technology
2013-01-01
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Series: | Iranica Journal of Energy and Environment |
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Online Access: | http://www.ijee.net/Journal/ijee/vol4/no1/9.pdf |
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author | Razieh Jabari seresht Mohsen Jahanshahi Ali Morad Rashidi Ali Asghar Ghoreyshi |
author_facet | Razieh Jabari seresht Mohsen Jahanshahi Ali Morad Rashidi Ali Asghar Ghoreyshi |
author_sort | Razieh Jabari seresht |
collection | DOAJ |
description | Thermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectroscopy. The result indicated that the reduced graphene at 900°C (GR900) had the highest quality in comparison with the other temperatures. Additionally, GR900 exhibited a sharp (002) peak corresponding to an interlayer distance of 3.39° A, which is close to that of conventional graphene (3.4°A). However, the structure of GR900 was also investigated by transmission electron microscopy (TEM), scanning electron microscopy (SEM) and the results supported the previous findings. |
first_indexed | 2024-04-24T15:36:33Z |
format | Article |
id | doaj.art-a53c424e039247b49b6807d046835c37 |
institution | Directory Open Access Journal |
issn | 2079-2115 2079-2123 |
language | English |
last_indexed | 2024-04-24T15:36:33Z |
publishDate | 2013-01-01 |
publisher | Babol Noshirvani University of Technology |
record_format | Article |
series | Iranica Journal of Energy and Environment |
spelling | doaj.art-a53c424e039247b49b6807d046835c372024-04-02T01:54:59ZengBabol Noshirvani University of TechnologyIranica Journal of Energy and Environment2079-21152079-21232013-01-0141535910.5829/idosi.ijee.2013.04.01.09Synthesis and Characterization of Thermally-Reduced GrapheneRazieh Jabari sereshtMohsen JahanshahiAli Morad RashidiAli Asghar GhoreyshiThermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectroscopy. The result indicated that the reduced graphene at 900°C (GR900) had the highest quality in comparison with the other temperatures. Additionally, GR900 exhibited a sharp (002) peak corresponding to an interlayer distance of 3.39° A, which is close to that of conventional graphene (3.4°A). However, the structure of GR900 was also investigated by transmission electron microscopy (TEM), scanning electron microscopy (SEM) and the results supported the previous findings.http://www.ijee.net/Journal/ijee/vol4/no1/9.pdfGrapheneGraphene oxideThermal reductionX-ray diffractionFTIR spectroscopyRaman spectroscopy |
spellingShingle | Razieh Jabari seresht Mohsen Jahanshahi Ali Morad Rashidi Ali Asghar Ghoreyshi Synthesis and Characterization of Thermally-Reduced Graphene Iranica Journal of Energy and Environment Graphene Graphene oxide Thermal reduction X-ray diffraction FTIR spectroscopy Raman spectroscopy |
title | Synthesis and Characterization of Thermally-Reduced Graphene |
title_full | Synthesis and Characterization of Thermally-Reduced Graphene |
title_fullStr | Synthesis and Characterization of Thermally-Reduced Graphene |
title_full_unstemmed | Synthesis and Characterization of Thermally-Reduced Graphene |
title_short | Synthesis and Characterization of Thermally-Reduced Graphene |
title_sort | synthesis and characterization of thermally reduced graphene |
topic | Graphene Graphene oxide Thermal reduction X-ray diffraction FTIR spectroscopy Raman spectroscopy |
url | http://www.ijee.net/Journal/ijee/vol4/no1/9.pdf |
work_keys_str_mv | AT raziehjabariseresht synthesisandcharacterizationofthermallyreducedgraphene AT mohsenjahanshahi synthesisandcharacterizationofthermallyreducedgraphene AT alimoradrashidi synthesisandcharacterizationofthermallyreducedgraphene AT aliasgharghoreyshi synthesisandcharacterizationofthermallyreducedgraphene |