Synthesis and Characterization of Thermally-Reduced Graphene

Thermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectrosc...

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Main Authors: Razieh Jabari seresht, Mohsen Jahanshahi, Ali Morad Rashidi, Ali Asghar Ghoreyshi
Format: Article
Language:English
Published: Babol Noshirvani University of Technology 2013-01-01
Series:Iranica Journal of Energy and Environment
Subjects:
Online Access:http://www.ijee.net/Journal/ijee/vol4/no1/9.pdf
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author Razieh Jabari seresht
Mohsen Jahanshahi
Ali Morad Rashidi
Ali Asghar Ghoreyshi
author_facet Razieh Jabari seresht
Mohsen Jahanshahi
Ali Morad Rashidi
Ali Asghar Ghoreyshi
author_sort Razieh Jabari seresht
collection DOAJ
description Thermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectroscopy. The result indicated that the reduced graphene at 900°C (GR900) had the highest quality in comparison with the other temperatures. Additionally, GR900 exhibited a sharp (002) peak corresponding to an interlayer distance of 3.39° A, which is close to that of conventional graphene (3.4°A). However, the structure of GR900 was also investigated by transmission electron microscopy (TEM), scanning electron microscopy (SEM) and the results supported the previous findings.
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spelling doaj.art-a53c424e039247b49b6807d046835c372024-04-02T01:54:59ZengBabol Noshirvani University of TechnologyIranica Journal of Energy and Environment2079-21152079-21232013-01-0141535910.5829/idosi.ijee.2013.04.01.09Synthesis and Characterization of Thermally-Reduced GrapheneRazieh Jabari sereshtMohsen JahanshahiAli Morad RashidiAli Asghar GhoreyshiThermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectroscopy. The result indicated that the reduced graphene at 900°C (GR900) had the highest quality in comparison with the other temperatures. Additionally, GR900 exhibited a sharp (002) peak corresponding to an interlayer distance of 3.39° A, which is close to that of conventional graphene (3.4°A). However, the structure of GR900 was also investigated by transmission electron microscopy (TEM), scanning electron microscopy (SEM) and the results supported the previous findings.http://www.ijee.net/Journal/ijee/vol4/no1/9.pdfGrapheneGraphene oxideThermal reductionX-ray diffractionFTIR spectroscopyRaman spectroscopy
spellingShingle Razieh Jabari seresht
Mohsen Jahanshahi
Ali Morad Rashidi
Ali Asghar Ghoreyshi
Synthesis and Characterization of Thermally-Reduced Graphene
Iranica Journal of Energy and Environment
Graphene
Graphene oxide
Thermal reduction
X-ray diffraction
FTIR spectroscopy
Raman spectroscopy
title Synthesis and Characterization of Thermally-Reduced Graphene
title_full Synthesis and Characterization of Thermally-Reduced Graphene
title_fullStr Synthesis and Characterization of Thermally-Reduced Graphene
title_full_unstemmed Synthesis and Characterization of Thermally-Reduced Graphene
title_short Synthesis and Characterization of Thermally-Reduced Graphene
title_sort synthesis and characterization of thermally reduced graphene
topic Graphene
Graphene oxide
Thermal reduction
X-ray diffraction
FTIR spectroscopy
Raman spectroscopy
url http://www.ijee.net/Journal/ijee/vol4/no1/9.pdf
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AT alimoradrashidi synthesisandcharacterizationofthermallyreducedgraphene
AT aliasgharghoreyshi synthesisandcharacterizationofthermallyreducedgraphene