Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques

Titania nanofibers were successfully synthesized by sol-gel coating of electrospun polymer nanofibers followed by calcining to form either the pure anatase or rutile phases. Characterization of these materials was carried out using scanning electron microscopy (SEM), transmission electron microscopy...

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Main Authors: Soo-Jin Park, Yong C. Kang, Ed A. Evans, Rex D. Ramsier, George G. Chase
Format: Article
Language:English
Published: SAGE Publishing 2010-03-01
Series:Journal of Engineered Fibers and Fabrics
Online Access:http://www.jeffjournal.org/papers/Volume5/5.1.6Chase2.pdf
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author Soo-Jin Park
Yong C. Kang
Ed A. Evans
Rex D. Ramsier
George G. Chase
author_facet Soo-Jin Park
Yong C. Kang
Ed A. Evans
Rex D. Ramsier
George G. Chase
author_sort Soo-Jin Park
collection DOAJ
description Titania nanofibers were successfully synthesized by sol-gel coating of electrospun polymer nanofibers followed by calcining to form either the pure anatase or rutile phases. Characterization of these materials was carried out using scanning electron microscopy (SEM), transmission electron microscopy (TEM), diffuse reflectance Fourier transform infrared spectroscopy (DRIFTS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and UV-vis spectroscopy techniques. The average diameter of these ceramic nanofibers was observed to be around 200 nm for both the rutile and anatase forms. The valence band structure and optical absorption thresholds differ, however, indicating that nano-fibrous mats of titania can be selectively developed for different applications in catalysis and photochemistry.
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spelling doaj.art-a54783d1b2e04430a0dc642d2e50aa5d2022-12-22T00:41:24ZengSAGE PublishingJournal of Engineered Fibers and Fabrics1558-92502010-03-01515056Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning TechniquesSoo-Jin ParkYong C. KangEd A. EvansRex D. RamsierGeorge G. ChaseTitania nanofibers were successfully synthesized by sol-gel coating of electrospun polymer nanofibers followed by calcining to form either the pure anatase or rutile phases. Characterization of these materials was carried out using scanning electron microscopy (SEM), transmission electron microscopy (TEM), diffuse reflectance Fourier transform infrared spectroscopy (DRIFTS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and UV-vis spectroscopy techniques. The average diameter of these ceramic nanofibers was observed to be around 200 nm for both the rutile and anatase forms. The valence band structure and optical absorption thresholds differ, however, indicating that nano-fibrous mats of titania can be selectively developed for different applications in catalysis and photochemistry.http://www.jeffjournal.org/papers/Volume5/5.1.6Chase2.pdf
spellingShingle Soo-Jin Park
Yong C. Kang
Ed A. Evans
Rex D. Ramsier
George G. Chase
Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
Journal of Engineered Fibers and Fabrics
title Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
title_full Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
title_fullStr Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
title_full_unstemmed Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
title_short Physical Characteristics of Titania Nanofibers Synthesized by Sol-Gel and Electrospinning Techniques
title_sort physical characteristics of titania nanofibers synthesized by sol gel and electrospinning techniques
url http://www.jeffjournal.org/papers/Volume5/5.1.6Chase2.pdf
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AT rexdramsier physicalcharacteristicsoftitaniananofiberssynthesizedbysolgelandelectrospinningtechniques
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