Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS)
<p class="orbitalabstract">The identification of cannabinoids directly in seeds is very controversial. According to the Recommended Methods for the Identification and Analysis of Cannabis and Cannabis products, “the seeds themselves do not contain Δ<sup>9</sup>-THC”. It i...
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Universidade Federal de Mato Grosso do Sul
2018-06-01
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Series: | Orbital: The Electronic Journal of Chemistry |
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Online Access: | http://orbital.ufms.br/index.php/Chemistry/article/view/1149 |
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author | Nayara A. dos Santos Rafael S. Ortiz Renata P. Limberger Valdemar Lacerda Júnior Wanderson Romão |
author_facet | Nayara A. dos Santos Rafael S. Ortiz Renata P. Limberger Valdemar Lacerda Júnior Wanderson Romão |
author_sort | Nayara A. dos Santos |
collection | DOAJ |
description | <p class="orbitalabstract">The identification of cannabinoids directly in seeds is very controversial. According to the Recommended Methods for the Identification and Analysis of Cannabis and Cannabis products, “the seeds themselves do not contain Δ<sup>9</sup>-THC”. It is defended the idea that the detection of Δ<sup>9</sup>-THC when it possibly occurs by contact of the seed with its bracts and/or flowers of the plant, which has a high content of this cannabinoid. In this paper, we reported a simple method of extraction and fast detection of Δ<sup>9</sup>-THC in the internal part of Cannabis seeds by negative-ion mode electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry (ESI(-)FT-ICR MS). Results showed that the method proposed allowed the chemotaxonomic forensic examination to prove the identification of Δ<sup>9</sup>-THC in Cannabis seeds.</p><p class="orbitalabstract"> </p><p class="orbitalabstract">DOI: <a href="http://dx.doi.org/10.17807/orbital.v10i5.1149">http://dx.doi.org/10.17807/orbital.v10i5.1149</a></p><p> </p> |
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issn | 1984-6428 |
language | English |
last_indexed | 2024-12-23T23:11:37Z |
publishDate | 2018-06-01 |
publisher | Universidade Federal de Mato Grosso do Sul |
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series | Orbital: The Electronic Journal of Chemistry |
spelling | doaj.art-a58edda5a03e4cf5a4e9b603e2d1d5ad2022-12-21T17:26:39ZengUniversidade Federal de Mato Grosso do SulOrbital: The Electronic Journal of Chemistry1984-64282018-06-0110538138510.17807/orbital.v10i5.1149513Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS)Nayara A. dos Santos0Rafael S. Ortiz1Renata P. Limberger2Valdemar Lacerda Júnior3Wanderson Romão4Laboratório de Petroleômica e Forense, Universidade Federal do Espírito Santo – Departamento de Química, CEP 29075910, Vitória, Espírito Santo, BrasilSuperintendência da Polícia Federal no Rio Grande do Sul, CEP 90130093, Porto Alegre, Rio Grande do Sul, BrasiFaculdade de Farmácia, Universidade Federal do Rio Grande do Sul, CEP 90610000, Porto Alegre, Rio Grande do Sul, BrasilChemistry Department Federal University of Espirito Santo Vitória, ES, BrazilInstituto Federal do Espírito Santo, IFES – Campus Vila Velha, CEP 29106010, Vila Velha, Espírito Santo Brasil<p class="orbitalabstract">The identification of cannabinoids directly in seeds is very controversial. According to the Recommended Methods for the Identification and Analysis of Cannabis and Cannabis products, “the seeds themselves do not contain Δ<sup>9</sup>-THC”. It is defended the idea that the detection of Δ<sup>9</sup>-THC when it possibly occurs by contact of the seed with its bracts and/or flowers of the plant, which has a high content of this cannabinoid. In this paper, we reported a simple method of extraction and fast detection of Δ<sup>9</sup>-THC in the internal part of Cannabis seeds by negative-ion mode electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry (ESI(-)FT-ICR MS). Results showed that the method proposed allowed the chemotaxonomic forensic examination to prove the identification of Δ<sup>9</sup>-THC in Cannabis seeds.</p><p class="orbitalabstract"> </p><p class="orbitalabstract">DOI: <a href="http://dx.doi.org/10.17807/orbital.v10i5.1149">http://dx.doi.org/10.17807/orbital.v10i5.1149</a></p><p> </p>http://orbital.ufms.br/index.php/Chemistry/article/view/1149cannabis seedsesi(-)ft-icrδ9-tetrahydrocannabinol |
spellingShingle | Nayara A. dos Santos Rafael S. Ortiz Renata P. Limberger Valdemar Lacerda Júnior Wanderson Romão Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) Orbital: The Electronic Journal of Chemistry cannabis seeds esi(-)ft-icr δ9-tetrahydrocannabinol |
title | Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) |
title_full | Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) |
title_fullStr | Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) |
title_full_unstemmed | Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) |
title_short | Identification of Δ9-Tetrahydrocannabinol (Δ9-THC) in Cannabis seeds by Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry (ESI(-)FT-ICR MS) |
title_sort | identification of δ9 tetrahydrocannabinol δ9 thc in cannabis seeds by electrospray ionization fourier transform ion cyclotron resonance mass spectrometry esi ft icr ms |
topic | cannabis seeds esi(-)ft-icr δ9-tetrahydrocannabinol |
url | http://orbital.ufms.br/index.php/Chemistry/article/view/1149 |
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