Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry

With easy-to-process 3D printing materials and fast production, the quality of dental services can be improved. In the conventional procedure, the dentist makes temporary crowns directly in the patient’s mouth, e.g., from the most commonly used bis-acrylic composites. Temporary crowns made directly...

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Main Authors: Marcel Firlej, Daniel Pieniak, Agata M. Niewczas, Agata Walczak, Ivo Domagała, Anna Borucka, Krzysztof Przystupa, Joanna Igielska-Kalwat, Wojciech Jarosz, Barbara Biedziak
Format: Article
Language:English
Published: MDPI AG 2021-08-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/16/4678
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author Marcel Firlej
Daniel Pieniak
Agata M. Niewczas
Agata Walczak
Ivo Domagała
Anna Borucka
Krzysztof Przystupa
Joanna Igielska-Kalwat
Wojciech Jarosz
Barbara Biedziak
author_facet Marcel Firlej
Daniel Pieniak
Agata M. Niewczas
Agata Walczak
Ivo Domagała
Anna Borucka
Krzysztof Przystupa
Joanna Igielska-Kalwat
Wojciech Jarosz
Barbara Biedziak
author_sort Marcel Firlej
collection DOAJ
description With easy-to-process 3D printing materials and fast production, the quality of dental services can be improved. In the conventional procedure, the dentist makes temporary crowns directly in the patient’s mouth, e.g., from the most commonly used bis-acrylic composites. Temporary crowns made directly in the office without the use of CAD/CAM are often of inferior quality, which directly results in impaired hygiene, poorer masticatory mechanics, greater deposition of plaque, calculus and sediment, and may adversely affect periodontal and gum health. The mechanical strength, resistance to aging and abrasion of 3D printing materials are higher than those of the soft materials used in conventional methods. This translates into durability. The patient leaves the surgery with a restoration of higher utility quality compared to the conventional method. The objective of the paper was to determine the influence of aging in artificial saliva of AM (additive manufacturing) orthodontic composites on their functional properties. For the purpose of the study, fillings well-known worldwide were selected. These were traditional UV-curable resins (M I, M II, M III, M V) and a hybrid material based on a UV-curable resin (M VI). Samples were stored in artificial saliva at 37 ± 1 °C in a thermal chamber for 6 months. Indentation hardness, frictional tests and sliding wear measurements were conducted. A comparison between various materials was made. Descriptive statistics, degradation coefficients, H<sup>2</sup>E, Archard wear and specific wear rate were calculated. The Weibull statistical test for indentation hardness was performed and Hertzian contact stresses for the frictional association were calculated for unaged (M I, M II, M III, M V, M VI) and aged (M I AS, M II AS, M III AS, M V AS, M VI AS) samples. M I exhibited the lowest average hardness among the unaged materials, while M III AS had the lowest average hardness among the aged materials. Comparably low hardness was demonstrated by the M I AS material. The coefficient of friction values for the aged samples were found to be higher. The lowest wear value was demonstrated by the M I material. The wear resistance of most of the tested materials deteriorated after aging. The M VI AS material had the highest increase in wear. According to the results provided, not only the chemical composition and structure, but also aging have a great impact on the indentation hardness and wear resistance of the tested orthodontic materials.
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spelling doaj.art-a5ec06ff17bb4a5cbd5efb09fbabcd502023-11-22T08:31:09ZengMDPI AGMaterials1996-19442021-08-011416467810.3390/ma14164678Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in DentistryMarcel Firlej0Daniel Pieniak1Agata M. Niewczas2Agata Walczak3Ivo Domagała4Anna Borucka5Krzysztof Przystupa6Joanna Igielska-Kalwat7Wojciech Jarosz8Barbara Biedziak9Department of Craniofacial Anomalies, Poznan University of Medical Sciences, Bukowska 70, 60-812 Poznan, PolandDepartment of Mechanics and Machine Building, University of Economics and Innovations in Lublin, Projektowa 4, 20-209 Lublin, PolandDepartament of Conservative Dentistry with Endodontics, Medical University of Lublin, W. Chodźki 6, 20-093 Lublin, PolandDepartament of Fire Technology the Main School of Fire Service, Faculty of Safety Engineering and Civil Protection, Slowackiego 52/54, 01-629 Warsaw, PolandDepartment of Craniofacial Anomalies, Poznan University of Medical Sciences, Bukowska 70, 60-812 Poznan, PolandFaculty of Security, Logistics and Management, Military University of Technology, gen. S. Kaliskiego 2, 00-908 Warsaw, PolandDepartment of Automation, Lublin University of Technology, Nadbystrzycka 36, 20-618 Lublin, PolandDepartment of Craniofacial Anomalies, Poznan University of Medical Sciences, Bukowska 70, 60-812 Poznan, PolandDepartament of Fire Technology the Main School of Fire Service, Faculty of Safety Engineering and Civil Protection, Slowackiego 52/54, 01-629 Warsaw, PolandDepartment of Craniofacial Anomalies, Poznan University of Medical Sciences, Bukowska 70, 60-812 Poznan, PolandWith easy-to-process 3D printing materials and fast production, the quality of dental services can be improved. In the conventional procedure, the dentist makes temporary crowns directly in the patient’s mouth, e.g., from the most commonly used bis-acrylic composites. Temporary crowns made directly in the office without the use of CAD/CAM are often of inferior quality, which directly results in impaired hygiene, poorer masticatory mechanics, greater deposition of plaque, calculus and sediment, and may adversely affect periodontal and gum health. The mechanical strength, resistance to aging and abrasion of 3D printing materials are higher than those of the soft materials used in conventional methods. This translates into durability. The patient leaves the surgery with a restoration of higher utility quality compared to the conventional method. The objective of the paper was to determine the influence of aging in artificial saliva of AM (additive manufacturing) orthodontic composites on their functional properties. For the purpose of the study, fillings well-known worldwide were selected. These were traditional UV-curable resins (M I, M II, M III, M V) and a hybrid material based on a UV-curable resin (M VI). Samples were stored in artificial saliva at 37 ± 1 °C in a thermal chamber for 6 months. Indentation hardness, frictional tests and sliding wear measurements were conducted. A comparison between various materials was made. Descriptive statistics, degradation coefficients, H<sup>2</sup>E, Archard wear and specific wear rate were calculated. The Weibull statistical test for indentation hardness was performed and Hertzian contact stresses for the frictional association were calculated for unaged (M I, M II, M III, M V, M VI) and aged (M I AS, M II AS, M III AS, M V AS, M VI AS) samples. M I exhibited the lowest average hardness among the unaged materials, while M III AS had the lowest average hardness among the aged materials. Comparably low hardness was demonstrated by the M I AS material. The coefficient of friction values for the aged samples were found to be higher. The lowest wear value was demonstrated by the M I material. The wear resistance of most of the tested materials deteriorated after aging. The M VI AS material had the highest increase in wear. According to the results provided, not only the chemical composition and structure, but also aging have a great impact on the indentation hardness and wear resistance of the tested orthodontic materials.https://www.mdpi.com/1996-1944/14/16/4678dental materialscompositesCAD/CAM3D printingartificial salivasliding wear
spellingShingle Marcel Firlej
Daniel Pieniak
Agata M. Niewczas
Agata Walczak
Ivo Domagała
Anna Borucka
Krzysztof Przystupa
Joanna Igielska-Kalwat
Wojciech Jarosz
Barbara Biedziak
Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
Materials
dental materials
composites
CAD/CAM
3D printing
artificial saliva
sliding wear
title Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
title_full Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
title_fullStr Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
title_full_unstemmed Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
title_short Effect of Artificial Aging on Mechanical and Tribological Properties of CAD/CAM Composite Materials Used in Dentistry
title_sort effect of artificial aging on mechanical and tribological properties of cad cam composite materials used in dentistry
topic dental materials
composites
CAD/CAM
3D printing
artificial saliva
sliding wear
url https://www.mdpi.com/1996-1944/14/16/4678
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