Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy

Accurate and non-destructive technology for detection of subsurface defect has become a key requirement with the emergence of various ultra-precision machining technologies and the application of ultra-precision components. The combination of acoustic technique for sub-surface detection and atomic f...

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Main Authors: Yuyang Wang, Chengjian Wu, Jinyan Tang, Mingyu Duan, Jian Chen, Bing-Feng Ju, Yuan-Liu Chen
Format: Article
Language:English
Published: MDPI AG 2022-05-01
Series:Applied Sciences
Subjects:
Online Access:https://www.mdpi.com/2076-3417/12/11/5460
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author Yuyang Wang
Chengjian Wu
Jinyan Tang
Mingyu Duan
Jian Chen
Bing-Feng Ju
Yuan-Liu Chen
author_facet Yuyang Wang
Chengjian Wu
Jinyan Tang
Mingyu Duan
Jian Chen
Bing-Feng Ju
Yuan-Liu Chen
author_sort Yuyang Wang
collection DOAJ
description Accurate and non-destructive technology for detection of subsurface defect has become a key requirement with the emergence of various ultra-precision machining technologies and the application of ultra-precision components. The combination of acoustic technique for sub-surface detection and atomic force microscopy (AFM) for measurement with high resolution is a potential method for studying the subsurface structure of workpiece. For this purpose, contact-resonance AFM (CR-AFM) is a typical technique. In this paper, a CR-AFM system with a different principle from commercially available instruments is set up and used for the detection of sub-surface Si samples with grating structures and covered by different thickness of highly oriented pyrolytic graphite (HOPG). The influence of subsurface burial depth on the detection capability is studied by simulations and experiments. The thickest HOPG film allowing for sub-surface measurement by the proposed method is verified to be about 30 μm, which is much larger than the feature size of the subsurface microstructure. The manuscript introduces the difference between this subsurface topography measurement principle and the commercially available AFM measurement principle, and analyzes its advantages and disadvantages. The experimental results demonstrates that the technique has the capability to reveal sub-surface microstructures with relatively large buried depth and is potential for engineering application in ultra-precision technologies.
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spelling doaj.art-a65226763bc24a87aa2123b3506233552023-11-23T13:42:05ZengMDPI AGApplied Sciences2076-34172022-05-011211546010.3390/app12115460Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force MicroscopyYuyang Wang0Chengjian Wu1Jinyan Tang2Mingyu Duan3Jian Chen4Bing-Feng Ju5Yuan-Liu Chen6State Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaState Key Lab of Fluid Power and Mechatronic Systems, School of Mechanical Engineering, Zhejiang University, Hangzhou 310027, ChinaAccurate and non-destructive technology for detection of subsurface defect has become a key requirement with the emergence of various ultra-precision machining technologies and the application of ultra-precision components. The combination of acoustic technique for sub-surface detection and atomic force microscopy (AFM) for measurement with high resolution is a potential method for studying the subsurface structure of workpiece. For this purpose, contact-resonance AFM (CR-AFM) is a typical technique. In this paper, a CR-AFM system with a different principle from commercially available instruments is set up and used for the detection of sub-surface Si samples with grating structures and covered by different thickness of highly oriented pyrolytic graphite (HOPG). The influence of subsurface burial depth on the detection capability is studied by simulations and experiments. The thickest HOPG film allowing for sub-surface measurement by the proposed method is verified to be about 30 μm, which is much larger than the feature size of the subsurface microstructure. The manuscript introduces the difference between this subsurface topography measurement principle and the commercially available AFM measurement principle, and analyzes its advantages and disadvantages. The experimental results demonstrates that the technique has the capability to reveal sub-surface microstructures with relatively large buried depth and is potential for engineering application in ultra-precision technologies.https://www.mdpi.com/2076-3417/12/11/5460measurementsub-surface microstructureultrasonic AFMcontact-resonance AFMburied depth
spellingShingle Yuyang Wang
Chengjian Wu
Jinyan Tang
Mingyu Duan
Jian Chen
Bing-Feng Ju
Yuan-Liu Chen
Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
Applied Sciences
measurement
sub-surface microstructure
ultrasonic AFM
contact-resonance AFM
buried depth
title Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
title_full Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
title_fullStr Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
title_full_unstemmed Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
title_short Measurement of Sub-Surface Microstructures Based on a Developed Ultrasonic Atomic Force Microscopy
title_sort measurement of sub surface microstructures based on a developed ultrasonic atomic force microscopy
topic measurement
sub-surface microstructure
ultrasonic AFM
contact-resonance AFM
buried depth
url https://www.mdpi.com/2076-3417/12/11/5460
work_keys_str_mv AT yuyangwang measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT chengjianwu measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT jinyantang measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT mingyuduan measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT jianchen measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT bingfengju measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy
AT yuanliuchen measurementofsubsurfacemicrostructuresbasedonadevelopedultrasonicatomicforcemicroscopy