rac-Ethyl (2Z)-3-{2-[(Z)-4-ethoxy-4-oxobut-2-en-2-ylamino]cyclohexylamino}but-2-enoate

The asymmetric unit of the title compound, C18H30N2O4, contains two independent molecules. In each molecule, the cyclohexane ring adopts a chair conformation with equatorial orientation of the substituents, and the conformation is stabilized by two intramolecular N—H...O hydrogen bonds...

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Bibliographic Details
Main Authors: Mohamed Anoir Harrad, Brahim Boualy, Mustapha Ait Ali, Larbi El Firdoussi, Corrado Rizzoli
Format: Article
Language:English
Published: International Union of Crystallography 2011-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811015248
Description
Summary:The asymmetric unit of the title compound, C18H30N2O4, contains two independent molecules. In each molecule, the cyclohexane ring adopts a chair conformation with equatorial orientation of the substituents, and the conformation is stabilized by two intramolecular N—H...O hydrogen bonds, forming rings of S(6) graph-set motif. One ethoxy group and one ethyl group are disordered over two sets of sites with refined occupancy ratios of 0.704 (2):0.296 (2) and 0.505 (3):0.495 (3), respectively. In the crystal, a weak intermolecular C—H...O hydrogen interaction is observed, involving the O atom of the major component of the disordered ethoxy group.
ISSN:1600-5368