双咪唑磺酸型离子液体催化煎炸废弃油制备生物柴油 Preparation of biodiesel from fried waste oil catalyzed by bisimidazole sulfonic acid type ionic liquid

双咪唑磺酸型离子液体催化煎炸废弃油制备生物柴油 Preparation of biodiesel from fried waste oil catalyzed by bisimidazole sulfonic acid type ionic liquid

为高效环保地制备生物柴油，通过三步法合成了一系列HSO4HSO3-C3\[MIM\]Cn\[MIM\]C3-HSO3HSO4(简写为CnMSS，n=2~6)双咪唑磺酸型离子液体，对其催化酯交换反应的性能进行了探究，并对离子活性最强的离子液体进行了核磁共振表征。以该离子液体为催化剂，通过单因素实验对三油酸甘油酯模型反应条件进行优化，并在此基础上采用正交实验优化煎炸废弃油制备生物柴油的工艺条件，同时对生物柴油产品进行了红外光谱和核磁共振表征。结果表明：离子液体C5MSS的催化性能最强；在醇油摩尔比18∶ 1、反应时间8 h、反应温度100 ℃、催化剂用量8%（以三油酸甘油酯质量计）条件下，油酸甲酯...

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Bibliographic Details
Main Author:	刘昕婷1，周姚红1，肖观秀1，吴苏琴1，黄建平2，熊万明2 LIU Xinting1, ZHOU Yaohong1, XIAO Guanxiu1, WU Suqin1, HUANG Jianping2, XIONG Wanming2
Format:	Article
Language:	English
Published:	中粮工科（西安）国际工程有限公司 2022-05-01
Series:	Zhongguo youzhi
Subjects:	废弃油；离子液体；双咪唑磺酸；生物柴油 waste oil; ionic liquid; bisimidazole sulfonic acid; biodiesel
Online Access:	http://tg.chinaoils.cn/ch/reader/create_pdf.aspx?file_no=20220507&year_id=2022&quarter_id=5&falg=1

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