Adhesion evaluation of dental ceramics sintered on novel titanium alloys

Metal-ceramics dental prosthetic restorations are clinically recommended for their advantages related to good esthetic features along with strength and long-term clinical use. Given the importance of the quality of the metalceramic (M-C) bond, the metal substructure analysis has a major importance t...

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Main Authors: Stefan Tudoran, Lucian Toma Ciocan, Bogdan Mihai Galbinasu, Ion Patrascu, Vlad Gabriel Vasilescu
Format: Article
Language:English
Published: Amaltea Medical Publishing House 2023-12-01
Series:Romanian Journal of Stomatology
Subjects:
Online Access:https://rjs.com.ro/articles/2023.4/RJS_2023_4_Art-02.pdf
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author Stefan Tudoran
Lucian Toma Ciocan
Bogdan Mihai Galbinasu
Ion Patrascu
Vlad Gabriel Vasilescu
author_facet Stefan Tudoran
Lucian Toma Ciocan
Bogdan Mihai Galbinasu
Ion Patrascu
Vlad Gabriel Vasilescu
author_sort Stefan Tudoran
collection DOAJ
description Metal-ceramics dental prosthetic restorations are clinically recommended for their advantages related to good esthetic features along with strength and long-term clinical use. Given the importance of the quality of the metalceramic (M-C) bond, the metal substructure analysis has a major importance to the quality of the manufactured dental prosthesis. In the present study was analyzed the behavior of experimentally developed novel titanium alloys (TiZr, TiZrNbTa) comparatively with other frequently used titanium alloys (e.g., Ti Cp, Ti6Al4V) designated for the technology of mixed prosthetic restorations. All samples were been plated, simultaneously in the same conditions, with the same titanium specific compatible ceramic plating material (Ti22 Noritake). The examination of the surface of both components was performed by scanning electron microscopy SEM) analysis and EDS analysis, which showed differences in the characteristics of the oxide layer formed, depending on the composition of the metal substructure. The evaluation of the alloy-ceramic adhesion was performed by mechanical tests, which attest to the fact that the adhesion and the quality of the bond between metal and ceramic depend on the thickness of the oxide films formed. The results showed the superiority of titanium novel titanium alloys (TiZr, TiZrNbTa), having highest hardness values, highest values of shear strength, a continuous thin oxide films, and consequently, a better metal-ceramic adhesion. Comparatively, less ductile titanium alloys (TiZrNbTa/Ti3) are generating lower adhesion forces with values above 30MPa in some samples justifying less predictable clinical results.
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spelling doaj.art-a85a1cb1cfc9439d9ef011390a6446622024-03-21T08:49:52ZengAmaltea Medical Publishing HouseRomanian Journal of Stomatology1843-08052069-60782023-12-0169421322210.37897/RJS.2023.4.2Adhesion evaluation of dental ceramics sintered on novel titanium alloysStefan Tudoran0Lucian Toma Ciocan1Bogdan Mihai Galbinasu2Ion Patrascu3Vlad Gabriel Vasilescu4Technology of dental prostheses, Faculty of Dentistry, “Carol Davila” University of Medicine and Pharmacy, Bucharest, RomaniaTechnology of dental prostheses, Faculty of Dentistry, “Carol Davila” University of Medicine and Pharmacy, Bucharest, RomaniaDiscipline Morphology of Teeth, Dental Arches and Dental Materials, Faculty of Dentistry, “Carol Davila” University of Medicine and Pharmacy, Bucharest, RomaniaTechnology of dental prostheses, Faculty of Dentistry, “Carol Davila” University of Medicine and Pharmacy, Bucharest, RomaniaTechnology of dental prostheses, Faculty of Dentistry, “Carol Davila” University of Medicine and Pharmacy, Bucharest, RomaniaMetal-ceramics dental prosthetic restorations are clinically recommended for their advantages related to good esthetic features along with strength and long-term clinical use. Given the importance of the quality of the metalceramic (M-C) bond, the metal substructure analysis has a major importance to the quality of the manufactured dental prosthesis. In the present study was analyzed the behavior of experimentally developed novel titanium alloys (TiZr, TiZrNbTa) comparatively with other frequently used titanium alloys (e.g., Ti Cp, Ti6Al4V) designated for the technology of mixed prosthetic restorations. All samples were been plated, simultaneously in the same conditions, with the same titanium specific compatible ceramic plating material (Ti22 Noritake). The examination of the surface of both components was performed by scanning electron microscopy SEM) analysis and EDS analysis, which showed differences in the characteristics of the oxide layer formed, depending on the composition of the metal substructure. The evaluation of the alloy-ceramic adhesion was performed by mechanical tests, which attest to the fact that the adhesion and the quality of the bond between metal and ceramic depend on the thickness of the oxide films formed. The results showed the superiority of titanium novel titanium alloys (TiZr, TiZrNbTa), having highest hardness values, highest values of shear strength, a continuous thin oxide films, and consequently, a better metal-ceramic adhesion. Comparatively, less ductile titanium alloys (TiZrNbTa/Ti3) are generating lower adhesion forces with values above 30MPa in some samples justifying less predictable clinical results.https://rjs.com.ro/articles/2023.4/RJS_2023_4_Art-02.pdftitanium alloysmetal-ceramic bond (m-c)interfaceoxide layereds analysismicroscopic analysis
spellingShingle Stefan Tudoran
Lucian Toma Ciocan
Bogdan Mihai Galbinasu
Ion Patrascu
Vlad Gabriel Vasilescu
Adhesion evaluation of dental ceramics sintered on novel titanium alloys
Romanian Journal of Stomatology
titanium alloys
metal-ceramic bond (m-c)
interface
oxide layer
eds analysis
microscopic analysis
title Adhesion evaluation of dental ceramics sintered on novel titanium alloys
title_full Adhesion evaluation of dental ceramics sintered on novel titanium alloys
title_fullStr Adhesion evaluation of dental ceramics sintered on novel titanium alloys
title_full_unstemmed Adhesion evaluation of dental ceramics sintered on novel titanium alloys
title_short Adhesion evaluation of dental ceramics sintered on novel titanium alloys
title_sort adhesion evaluation of dental ceramics sintered on novel titanium alloys
topic titanium alloys
metal-ceramic bond (m-c)
interface
oxide layer
eds analysis
microscopic analysis
url https://rjs.com.ro/articles/2023.4/RJS_2023_4_Art-02.pdf
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AT luciantomaciocan adhesionevaluationofdentalceramicssinteredonnoveltitaniumalloys
AT bogdanmihaigalbinasu adhesionevaluationofdentalceramicssinteredonnoveltitaniumalloys
AT ionpatrascu adhesionevaluationofdentalceramicssinteredonnoveltitaniumalloys
AT vladgabrielvasilescu adhesionevaluationofdentalceramicssinteredonnoveltitaniumalloys