Porous Biocoatings Based on Diatomite with Incorporated ZrO<sub>2</sub> Particles for Biodegradable Magnesium Implants

In the present work, the surface of a biodegradable Mg alloy was modified to create porous diatomite biocoatings using the method of micro-arc oxidation. The coatings were applied at process voltages in the range of 350–500 V. We have studied the influence of the addition of ZrO<sub>2</sub&...

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Bibliographic Details
Main Authors: Mariya B. Sedelnikova, Alexander D. Kashin, Pavel V. Uvarkin, Alexey I. Tolmachev, Yurii P. Sharkeev, Anna V. Ugodchikova, Nikita A. Luginin, Olga V. Bakina
Format: Article
Language:English
Published: MDPI AG 2023-04-01
Series:Journal of Functional Biomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4983/14/5/241
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Summary:In the present work, the surface of a biodegradable Mg alloy was modified to create porous diatomite biocoatings using the method of micro-arc oxidation. The coatings were applied at process voltages in the range of 350–500 V. We have studied the influence of the addition of ZrO<sub>2</sub> microparticles on the structure and properties of diatomite-based protective coatings for Mg implants. The structure and properties of the resulting coatings were examined using a number of research methods. It was found that the coatings have a porous structure and contain ZrO<sub>2</sub> particles. The coatings were mostly characterized by pores less than 1 μm in size. However, as the voltage of the MAO process increases, the number of larger pores (5–10 μm in size) also increases. However, the porosity of the coatings varied insignificantly and amounted to 5 ± 1%. It has been revealed that the incorporation of ZrO<sub>2</sub> particles substantially affects the properties of diatomite-based coatings. The adhesive strength of the coatings has increased by approximately 30%, and the corrosion resistance has increased by two orders of magnitude compared to the coatings without zirconia particles.
ISSN:2079-4983