A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors

Chemoresistive nanostructured gas sensors are employed in many diverse applications in the medical, industrial, environmental, etc. fields; therefore, it is crucial to have a device that is able to quickly calibrate and characterize them. To this aim, a portable, user-friendly device designed to eas...

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Main Authors: Michele Astolfi, Giulia Zonta, Sandro Gherardi, Cesare Malagù, Donato Vincenzi, Giorgio Rispoli
Format: Article
Language:English
Published: MDPI AG 2023-09-01
Series:Nanomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4991/13/18/2549
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author Michele Astolfi
Giulia Zonta
Sandro Gherardi
Cesare Malagù
Donato Vincenzi
Giorgio Rispoli
author_facet Michele Astolfi
Giulia Zonta
Sandro Gherardi
Cesare Malagù
Donato Vincenzi
Giorgio Rispoli
author_sort Michele Astolfi
collection DOAJ
description Chemoresistive nanostructured gas sensors are employed in many diverse applications in the medical, industrial, environmental, etc. fields; therefore, it is crucial to have a device that is able to quickly calibrate and characterize them. To this aim, a portable, user-friendly device designed to easily calibrate a sensor in laboratory and/or on field is introduced here. The device comprises a small hermetically sealed chamber (containing the sensor socket and a temperature/humidity sensor), a pneumatic system, and a custom electronics controlled by a Raspberry Pi 4 developing board, running a custom software (Version 1.0) whose user interface is accessed via a multitouch-screen. This device automatically characterizes the sensor heater in order to precisely set the desired working temperature, it acquires and plots the sensor current-to-voltage and Arrhenius relationships on the touch screen, and it can record the sensor responses to different gases and environments. These tests were performed in dry air on two representative sensors based on widely used SnO<sub>2</sub> material. The device demonstrated the independence of the Arrhenius plot from the film applied voltage and the linearity of the I–Vs, which resulted from the voltage step length (1–30 min) and temperature (200–550 °C).
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spelling doaj.art-aa5ee1740245447db329ae931a0bf7522023-11-19T12:14:32ZengMDPI AGNanomaterials2079-49912023-09-011318254910.3390/nano13182549A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based SensorsMichele Astolfi0Giulia Zonta1Sandro Gherardi2Cesare Malagù3Donato Vincenzi4Giorgio Rispoli5Department of Physics and Earth Science, University of Ferrara, 44122 Ferrara, ItalyDepartment of Physics and Earth Science, University of Ferrara, 44122 Ferrara, ItalySCENT S.r.l., 44124 Ferrara, ItalyDepartment of Physics and Earth Science, University of Ferrara, 44122 Ferrara, ItalyDepartment of Physics and Earth Science, University of Ferrara, 44122 Ferrara, ItalyDepartment of Neurosciences and Rehabilitation, University of Ferrara, 44121 Ferrara, ItalyChemoresistive nanostructured gas sensors are employed in many diverse applications in the medical, industrial, environmental, etc. fields; therefore, it is crucial to have a device that is able to quickly calibrate and characterize them. To this aim, a portable, user-friendly device designed to easily calibrate a sensor in laboratory and/or on field is introduced here. The device comprises a small hermetically sealed chamber (containing the sensor socket and a temperature/humidity sensor), a pneumatic system, and a custom electronics controlled by a Raspberry Pi 4 developing board, running a custom software (Version 1.0) whose user interface is accessed via a multitouch-screen. This device automatically characterizes the sensor heater in order to precisely set the desired working temperature, it acquires and plots the sensor current-to-voltage and Arrhenius relationships on the touch screen, and it can record the sensor responses to different gases and environments. These tests were performed in dry air on two representative sensors based on widely used SnO<sub>2</sub> material. The device demonstrated the independence of the Arrhenius plot from the film applied voltage and the linearity of the I–Vs, which resulted from the voltage step length (1–30 min) and temperature (200–550 °C).https://www.mdpi.com/2079-4991/13/18/2549gas sensorchemoresistivitysensor devicecurrent-voltage characteristicsArrhenius plotmetal-oxide
spellingShingle Michele Astolfi
Giulia Zonta
Sandro Gherardi
Cesare Malagù
Donato Vincenzi
Giorgio Rispoli
A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
Nanomaterials
gas sensor
chemoresistivity
sensor device
current-voltage characteristics
Arrhenius plot
metal-oxide
title A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
title_full A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
title_fullStr A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
title_full_unstemmed A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
title_short A Portable Device for I–V and Arrhenius Plots to Characterize Chemoresistive Gas Sensors: Test on SnO<sub>2</sub>-Based Sensors
title_sort portable device for i v and arrhenius plots to characterize chemoresistive gas sensors test on sno sub 2 sub based sensors
topic gas sensor
chemoresistivity
sensor device
current-voltage characteristics
Arrhenius plot
metal-oxide
url https://www.mdpi.com/2079-4991/13/18/2549
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