Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid

<p>A simple procedure for synthesis of chitosan-coated magnetic microparticles (CMMP) using glutaraldehyde as a cross-linker and polyethylene glycol (PEG) as a spacer arm has been developed. The functionalized microparticles were prepared using an inexpensive, simple, rapid, one-pot process, b...

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Main Authors: Uripto Trisno Santoso, Rodiansono Rodiansono, Budi Junaidi, Dewi Umaningrum
Format: Article
Language:English
Published: Universitas Lambung Mangkurat 2015-07-01
Series:Journal of Wetlands Environmental Management
Subjects:
Online Access:http://ijwem.unlam.ac.id/index.php/ijwem/article/view/43
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author Uripto Trisno Santoso
Rodiansono Rodiansono
Budi Junaidi
Dewi Umaningrum
author_facet Uripto Trisno Santoso
Rodiansono Rodiansono
Budi Junaidi
Dewi Umaningrum
author_sort Uripto Trisno Santoso
collection DOAJ
description <p>A simple procedure for synthesis of chitosan-coated magnetic microparticles (CMMP) using glutaraldehyde as a cross-linker and polyethylene glycol (PEG) as a spacer arm has been developed. The functionalized microparticles were prepared using an inexpensive, simple, rapid, one-pot process, based on the heating of chitosan, PEG, and ferrous sulfate mixture at high pH. X-ray diffraction results indicated that the surface-modified Fe<sub>3</sub>O<sub>4</sub> microparticles did not lead to phase change unlike the pure Fe<sub>3</sub>O<sub>4</sub>. Magnetic chitosan adsorbent has been evaluated for removal of peat humic acid from its aqueous solution.</p>
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spelling doaj.art-ab06be6b82dc49f5bf37e603f9807bb32022-12-22T00:15:55ZengUniversitas Lambung MangkuratJournal of Wetlands Environmental Management2354-58442015-07-013132Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic AcidUripto Trisno Santoso0Rodiansono Rodiansono1Budi Junaidi2Dewi Umaningrum3Department of Chemistry, Faculty of Mathematics and natural Sciences, Lambung Mangkurat UniversityDepartement of Chemistry, Faculty of Mathematics and Natural Sciences, Lambung Mangkurat UniversityDepartement of Chemistry, Faculty of Mathematics and Natural Sciences, Lambung Mangkurat UniversityDepartement of Chemistry, Faculty of Mathematics and Natural Sciences, Lambung Mangkurat University<p>A simple procedure for synthesis of chitosan-coated magnetic microparticles (CMMP) using glutaraldehyde as a cross-linker and polyethylene glycol (PEG) as a spacer arm has been developed. The functionalized microparticles were prepared using an inexpensive, simple, rapid, one-pot process, based on the heating of chitosan, PEG, and ferrous sulfate mixture at high pH. X-ray diffraction results indicated that the surface-modified Fe<sub>3</sub>O<sub>4</sub> microparticles did not lead to phase change unlike the pure Fe<sub>3</sub>O<sub>4</sub>. Magnetic chitosan adsorbent has been evaluated for removal of peat humic acid from its aqueous solution.</p>http://ijwem.unlam.ac.id/index.php/ijwem/article/view/43chitosan, magnetic, microparticles, adsorption, humic acid, peat
spellingShingle Uripto Trisno Santoso
Rodiansono Rodiansono
Budi Junaidi
Dewi Umaningrum
Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
Journal of Wetlands Environmental Management
chitosan, magnetic, microparticles, adsorption, humic acid, peat
title Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
title_full Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
title_fullStr Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
title_full_unstemmed Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
title_short Synthesis of Chitosan-Coated Magnetic Microparticle Using Glutaraldehyde as Crosslinker and PEG as Spacer Arm and Its Application as Adsorbent of Peat Humic Acid
title_sort synthesis of chitosan coated magnetic microparticle using glutaraldehyde as crosslinker and peg as spacer arm and its application as adsorbent of peat humic acid
topic chitosan, magnetic, microparticles, adsorption, humic acid, peat
url http://ijwem.unlam.ac.id/index.php/ijwem/article/view/43
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AT budijunaidi synthesisofchitosancoatedmagneticmicroparticleusingglutaraldehydeascrosslinkerandpegasspacerarmanditsapplicationasadsorbentofpeathumicacid
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