Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions
Bismuth chalcogenides (Bi2X3, X = S, Se, Te) were synthesized from the elements under hydrothermal condition. Single phases of Bi2S3 and Bi2Se3 were produced at 240 °C. Bi2Te3 was obtained as an almost single phase with a small amount of Bi2TeO5. From the results of control experiments without water...
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Taylor & Francis Group
2014-12-01
|
Series: | Journal of Asian Ceramic Societies |
Subjects: | |
Online Access: | http://www.sciencedirect.com/science/article/pii/S2187076414000852 |
_version_ | 1831690237048258560 |
---|---|
author | Keitaro Tezuka Saori Kase Yue Jin Shan |
author_facet | Keitaro Tezuka Saori Kase Yue Jin Shan |
author_sort | Keitaro Tezuka |
collection | DOAJ |
description | Bismuth chalcogenides (Bi2X3, X = S, Se, Te) were synthesized from the elements under hydrothermal condition. Single phases of Bi2S3 and Bi2Se3 were produced at 240 °C. Bi2Te3 was obtained as an almost single phase with a small amount of Bi2TeO5. From the results of control experiments without water, the hydrothermal condition in the production of Bi2S3 was more effective than that of Bi2Se3. The particles of obtained Bi2S3 were spherical, with a diameter of ∼1 μm. The Bi2Se3 particles were in a plate-like form, with a width of ∼1 μm and a thickness of ∼0.2 μm. |
first_indexed | 2024-12-20T11:09:11Z |
format | Article |
id | doaj.art-ab2eea7d2c52466a84e8fe591cc5a03a |
institution | Directory Open Access Journal |
issn | 2187-0764 |
language | English |
last_indexed | 2024-12-20T11:09:11Z |
publishDate | 2014-12-01 |
publisher | Taylor & Francis Group |
record_format | Article |
series | Journal of Asian Ceramic Societies |
spelling | doaj.art-ab2eea7d2c52466a84e8fe591cc5a03a2022-12-21T19:42:51ZengTaylor & Francis GroupJournal of Asian Ceramic Societies2187-07642014-12-012436637010.1016/j.jascer.2014.07.009Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditionsKeitaro TezukaSaori KaseYue Jin ShanBismuth chalcogenides (Bi2X3, X = S, Se, Te) were synthesized from the elements under hydrothermal condition. Single phases of Bi2S3 and Bi2Se3 were produced at 240 °C. Bi2Te3 was obtained as an almost single phase with a small amount of Bi2TeO5. From the results of control experiments without water, the hydrothermal condition in the production of Bi2S3 was more effective than that of Bi2Se3. The particles of obtained Bi2S3 were spherical, with a diameter of ∼1 μm. The Bi2Se3 particles were in a plate-like form, with a width of ∼1 μm and a thickness of ∼0.2 μm.http://www.sciencedirect.com/science/article/pii/S2187076414000852Hydrothermal reactionBismuthChalcogenideX-ray methods |
spellingShingle | Keitaro Tezuka Saori Kase Yue Jin Shan Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions Journal of Asian Ceramic Societies Hydrothermal reaction Bismuth Chalcogenide X-ray methods |
title | Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions |
title_full | Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions |
title_fullStr | Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions |
title_full_unstemmed | Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions |
title_short | Syntheses of Bi2X3 (X = S, Se, Te) from elements under hydrothermal conditions |
title_sort | syntheses of bi2x3 x s se te from elements under hydrothermal conditions |
topic | Hydrothermal reaction Bismuth Chalcogenide X-ray methods |
url | http://www.sciencedirect.com/science/article/pii/S2187076414000852 |
work_keys_str_mv | AT keitarotezuka synthesesofbi2x3xssetefromelementsunderhydrothermalconditions AT saorikase synthesesofbi2x3xssetefromelementsunderhydrothermalconditions AT yuejinshan synthesesofbi2x3xssetefromelementsunderhydrothermalconditions |