Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究)
建立了液相色谱-串联质谱测定小走中9种氨基甲酸酯类农药的多残留检测方法.样品经乙腈提取，中性氧化铝填充柱净化，然后采用HPLC-ESI( + )-MS/MS测定.着重探讨了液质联用体系的稳定性、测定中普遍存在的基体效应及其校正的可能方法.结果表明，本研究建立的方法简便、快捷、准确，适合大批量样品的测定....
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| Format: | Article |
| Language: | zho |
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Zhejiang University Press
2007-07-01
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| Series: | Zhejiang Daxue xuebao. Lixue ban |
| Subjects: | |
| Online Access: | https://doi.org/zjup/1008-9497.2007.34.4.426-431 |
| _version_ | 1797236248561057792 |
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| author | HUBei-zhen(胡贝贞) GUOWei-qiang(郭伟强) CHENXiao-mei(陈笑梅) |
| author_facet | HUBei-zhen(胡贝贞) GUOWei-qiang(郭伟强) CHENXiao-mei(陈笑梅) |
| author_sort | HUBei-zhen(胡贝贞) |
| collection | DOAJ |
| description | 建立了液相色谱-串联质谱测定小走中9种氨基甲酸酯类农药的多残留检测方法.样品经乙腈提取，中性氧化铝填充柱净化，然后采用HPLC-ESI( + )-MS/MS测定.着重探讨了液质联用体系的稳定性、测定中普遍存在的基体效应及其校正的可能方法.结果表明，本研究建立的方法简便、快捷、准确，适合大批量样品的测定. |
| first_indexed | 2024-04-24T17:00:50Z |
| format | Article |
| id | doaj.art-abb72b6fa86547369669aa404c0241dc |
| institution | Directory Open Access Journal |
| issn | 1008-9497 |
| language | zho |
| last_indexed | 2024-04-24T17:00:50Z |
| publishDate | 2007-07-01 |
| publisher | Zhejiang University Press |
| record_format | Article |
| series | Zhejiang Daxue xuebao. Lixue ban |
| spelling | doaj.art-abb72b6fa86547369669aa404c0241dc2024-03-29T01:58:24ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972007-07-01344426431zjup/1008-9497.2007.34.4.426-431Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究)HUBei-zhen(胡贝贞)0GUOWei-qiang(郭伟强)1CHENXiao-mei(陈笑梅)2 1.Department of Chemistry, Zhejiang University, Hangzhou 310028, China( 1.浙江大学化学系，浙江 杭州 310028) 1.Department of Chemistry, Zhejiang University, Hangzhou 310028, China( 1.浙江大学化学系，浙江 杭州 310028) 2.Zhejiang Entry-Exit Inspection and Quarantine Bureau, Hangzhou 310012, China( 2.浙江省出入境检验检疫局，浙江 杭州 310012)建立了液相色谱-串联质谱测定小走中9种氨基甲酸酯类农药的多残留检测方法.样品经乙腈提取，中性氧化铝填充柱净化，然后采用HPLC-ESI( + )-MS/MS测定.着重探讨了液质联用体系的稳定性、测定中普遍存在的基体效应及其校正的可能方法.结果表明，本研究建立的方法简便、快捷、准确，适合大批量样品的测定.https://doi.org/zjup/1008-9497.2007.34.4.426-431小麦氨基甲酸酯基体效应液相色谱-串联质谱 |
| spellingShingle | HUBei-zhen(胡贝贞) GUOWei-qiang(郭伟强) CHENXiao-mei(陈笑梅) Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) Zhejiang Daxue xuebao. Lixue ban 小麦 氨基甲酸酯 基体效应 液相色谱-串联质谱 |
| title | Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) |
| title_full | Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) |
| title_fullStr | Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) |
| title_full_unstemmed | Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) |
| title_short | Study of HPLC-MS/MS method for determination of carbmate pesticides in wheat samples(小麦中氨基甲酸酯类农药残留的HPLC-MS/MS测定方法研究) |
| title_sort | study of hplc ms ms method for determination of carbmate pesticides in wheat samples 小麦中氨基甲酸酯类农药残留的hplc ms ms测定方法研究 |
| topic | 小麦 氨基甲酸酯 基体效应 液相色谱-串联质谱 |
| url | https://doi.org/zjup/1008-9497.2007.34.4.426-431 |
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