Benzo[b]thiophene-2-carbaldehyde
A novel expedient synthesis of benzo[b]thiophene-2-carbaldehyde 2 is reported. It is based on the one-pot sequential reaction of methylthiobenzene 1 with BuLi and DMF to give 2 in 80% isolated yield.
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
MDPI AG
2014-05-01
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| Series: | Molbank |
| Subjects: | |
| Online Access: | http://www.mdpi.com/1422-8599/2014/2/M823 |
| _version_ | 1818540602207240192 |
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| author | Raffaella Mancuso Bartolo Gabriele |
| author_facet | Raffaella Mancuso Bartolo Gabriele |
| author_sort | Raffaella Mancuso |
| collection | DOAJ |
| description | A novel expedient synthesis of benzo[b]thiophene-2-carbaldehyde 2 is reported. It is based on the one-pot sequential reaction of methylthiobenzene 1 with BuLi and DMF to give 2 in 80% isolated yield. |
| first_indexed | 2024-12-11T21:57:32Z |
| format | Article |
| id | doaj.art-abbe53442f8247c7bc31c4ce2bf4a0ea |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-12-11T21:57:32Z |
| publishDate | 2014-05-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-abbe53442f8247c7bc31c4ce2bf4a0ea2022-12-22T00:49:15ZengMDPI AGMolbank1422-85992014-05-0120142M82310.3390/M823M823Benzo[b]thiophene-2-carbaldehydeRaffaella Mancuso0Bartolo Gabriele1Dipartimento di Chimica e Tecnologie Chimiche, Università della Calabria, Ponte Pietro Bucci 12/C, 87036 Arcavacata di Rende (CS), ItalyDipartimento di Chimica e Tecnologie Chimiche, Università della Calabria, Ponte Pietro Bucci 12/C, 87036 Arcavacata di Rende (CS), ItalyA novel expedient synthesis of benzo[b]thiophene-2-carbaldehyde 2 is reported. It is based on the one-pot sequential reaction of methylthiobenzene 1 with BuLi and DMF to give 2 in 80% isolated yield.http://www.mdpi.com/1422-8599/2014/2/M823benzo[b]thiophene-2-carbaldehydeformylationheterocyclization |
| spellingShingle | Raffaella Mancuso Bartolo Gabriele Benzo[b]thiophene-2-carbaldehyde Molbank benzo[b]thiophene-2-carbaldehyde formylation heterocyclization |
| title | Benzo[b]thiophene-2-carbaldehyde |
| title_full | Benzo[b]thiophene-2-carbaldehyde |
| title_fullStr | Benzo[b]thiophene-2-carbaldehyde |
| title_full_unstemmed | Benzo[b]thiophene-2-carbaldehyde |
| title_short | Benzo[b]thiophene-2-carbaldehyde |
| title_sort | benzo b thiophene 2 carbaldehyde |
| topic | benzo[b]thiophene-2-carbaldehyde formylation heterocyclization |
| url | http://www.mdpi.com/1422-8599/2014/2/M823 |
| work_keys_str_mv | AT raffaellamancuso benzobthiophene2carbaldehyde AT bartologabriele benzobthiophene2carbaldehyde |