Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method
Preventing the formation of the pyrochlore phase in the synthesis of PZN-PT powders requires controlling calcination parameters such as temperature, soaking time and atmosphere. These parameters were examined extensively to determine the time and temperature at which the perovskite phase is the majo...
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Elsevier
2017-01-01
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| Series: | Boletín de la Sociedad Española de Cerámica y Vidrio |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S0366317516300164 |
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| author | C.F.V. Raigoza D. Garcia J.A. Eiras R.H.G.A. Kiminami |
| author_facet | C.F.V. Raigoza D. Garcia J.A. Eiras R.H.G.A. Kiminami |
| author_sort | C.F.V. Raigoza |
| collection | DOAJ |
| description | Preventing the formation of the pyrochlore phase in the synthesis of PZN-PT powders requires controlling calcination parameters such as temperature, soaking time and atmosphere. These parameters were examined extensively to determine the time and temperature at which the perovskite phase is the majority phase, as well as the atmosphere that facilitates the formation of this phase. A maximum of 74% of perovskite phase was obtained under the following conditions: 1000 °C, 4 h in nitrogen atmosphere. In this work, we studied the influence of these parameters, which were optimized, on the formation the perovskite phase in PZN-10PT powders synthesized by the conventional solid state method. |
| first_indexed | 2024-12-22T17:17:22Z |
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| id | doaj.art-aceb8cb560e94620820881f6b6c0d968 |
| institution | Directory Open Access Journal |
| issn | 0366-3175 |
| language | English |
| last_indexed | 2024-12-22T17:17:22Z |
| publishDate | 2017-01-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Boletín de la Sociedad Española de Cerámica y Vidrio |
| spelling | doaj.art-aceb8cb560e94620820881f6b6c0d9682022-12-21T18:18:55ZengElsevierBoletín de la Sociedad Española de Cerámica y Vidrio0366-31752017-01-01561131810.1016/j.bsecv.2016.03.002Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides methodC.F.V. Raigoza0D. Garcia1J.A. Eiras2R.H.G.A. Kiminami3Universidad del Cauca, Departamento de Física, Grupo de Ciencia y Tecnología de Materiales Cerámicos (CYTEMAC), Popayán, ColombiaFederal University of São Carlos, Department of Physics, São Carlos, SP 13565-905, BrazilFederal University of São Carlos, Department of Physics, São Carlos, SP 13565-905, BrazilFederal University of São Carlos, Department of Materials Engineering, São Carlos, SP 13565-905, BrazilPreventing the formation of the pyrochlore phase in the synthesis of PZN-PT powders requires controlling calcination parameters such as temperature, soaking time and atmosphere. These parameters were examined extensively to determine the time and temperature at which the perovskite phase is the majority phase, as well as the atmosphere that facilitates the formation of this phase. A maximum of 74% of perovskite phase was obtained under the following conditions: 1000 °C, 4 h in nitrogen atmosphere. In this work, we studied the influence of these parameters, which were optimized, on the formation the perovskite phase in PZN-10PT powders synthesized by the conventional solid state method.http://www.sciencedirect.com/science/article/pii/S0366317516300164PZN-PTPerovskitePyrochlorePhase transformationTemperatureSoaking timeAtmosphere |
| spellingShingle | C.F.V. Raigoza D. Garcia J.A. Eiras R.H.G.A. Kiminami Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method Boletín de la Sociedad Española de Cerámica y Vidrio PZN-PT Perovskite Pyrochlore Phase transformation Temperature Soaking time Atmosphere |
| title | Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method |
| title_full | Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method |
| title_fullStr | Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method |
| title_full_unstemmed | Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method |
| title_short | Optimization of parameters in the synthesis of 0.90Pb(Zn1/3Nb2/3)O3–0.10PbTiO3 (PZN-10PT) powders obtained by the mixed oxides method |
| title_sort | optimization of parameters in the synthesis of 0 90pb zn1 3nb2 3 o3 0 10pbtio3 pzn 10pt powders obtained by the mixed oxides method |
| topic | PZN-PT Perovskite Pyrochlore Phase transformation Temperature Soaking time Atmosphere |
| url | http://www.sciencedirect.com/science/article/pii/S0366317516300164 |
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