| Summary: | We investigated the effect of different sintering temperatures ranging from 200<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo> </mo><mrow><mo>°</mo><mi mathvariant="normal">C</mi></mrow></mrow></semantics></math></inline-formula> to 600<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo> </mo><mrow><mo>°</mo><mi mathvariant="normal">C</mi></mrow></mrow></semantics></math></inline-formula> on the porous properties and pore microstructure of large capillary pressure wicks made of carbonyl nickel powder. The evolution model of hydraulic diameter was established and verified by the maximum pore diameter. Hydraulic diameter changed as the roughness of particle surfaces decreased and sintering necks grew large during sintering. In the contact-formation stage and the initial sintering stage (200–500<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo> </mo><mrow><mo>°</mo><mi mathvariant="normal">C</mi></mrow></mrow></semantics></math></inline-formula>), the decrease in the roughness of particle surfaces played a decisive role, contributing to an increase in hydraulic diameter. In the intermediate sintering stage (600<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo> </mo><mrow><mo>°</mo><mi mathvariant="normal">C</mi></mrow></mrow></semantics></math></inline-formula>), the growth of sintering necks dominated the process, however the hydraulic diameter was reduced. These results show that the maximum pore diameter first increased and then decreased in the same way as our evolution model. Permeability and capillary performance of the wicks first increased and then declined with increasing sintering temperature. We found the optimal sintering temperature to be 400<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo> </mo><mrow><mo>°</mo><mi mathvariant="normal">C</mi></mrow></mrow></semantics></math></inline-formula>, at which point the wicks achieved the maximum pore diameter of 1.21 μm, a permeability of 1.77 × 10<sup>−14</sup> m<sup>2</sup>, and their highest capillary performance of 1.46 × 10<sup>−8</sup> m.
|
|---|