Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments

The aim of this work was to show the evolution over time of the dynamic moduli in components made of Polybutylene Terephthalate reinforced with glass fiber when they are held to temperatures close to the glass transition temperature over time. For this purpose, PBT samples reinforced with short, gla...

Full description

Bibliographic Details
Main Authors: Carmelo Gómez, Jorge Mira, F.J. Carrión-Vilches, Francisco Cavas
Format: Article
Language:English
Published: MDPI AG 2021-01-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/3/483
_version_ 1797409199379972096
author Carmelo Gómez
Jorge Mira
F.J. Carrión-Vilches
Francisco Cavas
author_facet Carmelo Gómez
Jorge Mira
F.J. Carrión-Vilches
Francisco Cavas
author_sort Carmelo Gómez
collection DOAJ
description The aim of this work was to show the evolution over time of the dynamic moduli in components made of Polybutylene Terephthalate reinforced with glass fiber when they are held to temperatures close to the glass transition temperature over time. For this purpose, PBT samples reinforced with short, glass fibers of Ultradur<sup>®</sup> material with 0%, 20%, and 50% in weight content were tested. Dynamic moduli showed an increment with glass fiber content showing a nonlinear behavior with the temperature. The evolution of storage modulus was depicted by means of a modified law of mixtures with an effectiveness factor depending on temperature and fiber content, whereas the evolution over time was obtained with a time–temperature transformation generated with the TTS Data Analysis software of TA-instruments for a given temperature. Storage modulus showed a linear relationship with glass fiber content when components were held to temperatures near to their respective glass transition temperature, obtained from the maximum of loss modulus curve with temperature. In summary, the value and evolution of dynamic moduli of PBT samples improved with glass fiber content, allowing us to increase the durability of components when they are submitted to high-temperature environments.
first_indexed 2024-03-09T04:10:54Z
format Article
id doaj.art-aff8a5fd9a354405ad98694ec1980432
institution Directory Open Access Journal
issn 1996-1944
language English
last_indexed 2024-03-09T04:10:54Z
publishDate 2021-01-01
publisher MDPI AG
record_format Article
series Materials
spelling doaj.art-aff8a5fd9a354405ad98694ec19804322023-12-03T14:00:43ZengMDPI AGMaterials1996-19442021-01-0114348310.3390/ma14030483Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature EnvironmentsCarmelo Gómez0Jorge Mira1F.J. Carrión-Vilches2Francisco Cavas3Doctorate Program in Industrial Technologies, International School of Doctorate, Technical University of Cartagena, 30202 Cartagena, SpainDoctorate Program in Industrial Technologies, International School of Doctorate, Technical University of Cartagena, 30202 Cartagena, SpainMaterials Science and Metallurgical Engineering Group, Materials Engineering and Manufacturing Department, Technical University of Cartagena, 30202 Cartagena, SpainDepartment of Structures, Construction and Graphical Expression, Technical University of Cartagena, 30202 Cartagena, SpainThe aim of this work was to show the evolution over time of the dynamic moduli in components made of Polybutylene Terephthalate reinforced with glass fiber when they are held to temperatures close to the glass transition temperature over time. For this purpose, PBT samples reinforced with short, glass fibers of Ultradur<sup>®</sup> material with 0%, 20%, and 50% in weight content were tested. Dynamic moduli showed an increment with glass fiber content showing a nonlinear behavior with the temperature. The evolution of storage modulus was depicted by means of a modified law of mixtures with an effectiveness factor depending on temperature and fiber content, whereas the evolution over time was obtained with a time–temperature transformation generated with the TTS Data Analysis software of TA-instruments for a given temperature. Storage modulus showed a linear relationship with glass fiber content when components were held to temperatures near to their respective glass transition temperature, obtained from the maximum of loss modulus curve with temperature. In summary, the value and evolution of dynamic moduli of PBT samples improved with glass fiber content, allowing us to increase the durability of components when they are submitted to high-temperature environments.https://www.mdpi.com/1996-1944/14/3/483polymer compositesstorage modulusglass fiberhigh temperature
spellingShingle Carmelo Gómez
Jorge Mira
F.J. Carrión-Vilches
Francisco Cavas
Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
Materials
polymer composites
storage modulus
glass fiber
high temperature
title Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
title_full Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
title_fullStr Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
title_full_unstemmed Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
title_short Dynamic Moduli of Polybutylene Terephthalate Glass Fiber Reinforced in High-Temperature Environments
title_sort dynamic moduli of polybutylene terephthalate glass fiber reinforced in high temperature environments
topic polymer composites
storage modulus
glass fiber
high temperature
url https://www.mdpi.com/1996-1944/14/3/483
work_keys_str_mv AT carmelogomez dynamicmoduliofpolybutyleneterephthalateglassfiberreinforcedinhightemperatureenvironments
AT jorgemira dynamicmoduliofpolybutyleneterephthalateglassfiberreinforcedinhightemperatureenvironments
AT fjcarrionvilches dynamicmoduliofpolybutyleneterephthalateglassfiberreinforcedinhightemperatureenvironments
AT franciscocavas dynamicmoduliofpolybutyleneterephthalateglassfiberreinforcedinhightemperatureenvironments