Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy

High-entropy alloys (HEAs) have attracted extensive interest due to their unprecedented structure and mechanical performance. We recently proposed a series of novel corich twinning induced plasticity (TWIP) and transformation induced plasticity (TRIP) HEAs with superior tensile properties at room te...

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Main Authors: Hailong Yi, Daixiu Wei, Renyi Xie, Yifan Zhang, Hidemi Kato
Format: Article
Language:English
Published: MDPI AG 2021-03-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/14/5/1196
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author Hailong Yi
Daixiu Wei
Renyi Xie
Yifan Zhang
Hidemi Kato
author_facet Hailong Yi
Daixiu Wei
Renyi Xie
Yifan Zhang
Hidemi Kato
author_sort Hailong Yi
collection DOAJ
description High-entropy alloys (HEAs) have attracted extensive interest due to their unprecedented structure and mechanical performance. We recently proposed a series of novel corich twinning induced plasticity (TWIP) and transformation induced plasticity (TRIP) HEAs with superior tensile properties at room temperature; however, the hot deformation behavior has not been reported. Here, we investigated the dynamic recrystallization behavior and grain refinement of a representative TRIP-HEA, compressed at temperatures of 1123–1273 K with strain rates of 0.1–0.001 s<sup>−1</sup>. We characterized the impact of the temperature and strain rate on the grain structure evolution. A constitutive equation was constructed to reveal the correlations between the flow stress, strain rate, temperature, and strain. The apparent activation energy was estimated to be ~385.7 kJ/mol. The discontinuous dynamic recrystallization played an important role in the grain refinement, particularly at a relatively higher temperature and a lower strain rate, and the volume fraction and morphology of the recrystallized grains exhibited a strong dependency on the Zener–Hollomon parameter. The study provides guidelines for the grain refinement of HEAs through thermomechanical processing.
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spelling doaj.art-b0c8c715e598411cacad863893f5fddc2023-12-03T12:27:42ZengMDPI AGMaterials1996-19442021-03-01145119610.3390/ma14051196Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy AlloyHailong Yi0Daixiu Wei1Renyi Xie2Yifan Zhang3Hidemi Kato4State Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, ChinaInstitute for Materials Research, Tohoku University, 2-1-1 Katahira, Sendai 980-8577, Miyagi, JapanState Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, ChinaState Key Laboratory of Rolling and Automation, Northeastern University, Shenyang 110819, ChinaInstitute for Materials Research, Tohoku University, 2-1-1 Katahira, Sendai 980-8577, Miyagi, JapanHigh-entropy alloys (HEAs) have attracted extensive interest due to their unprecedented structure and mechanical performance. We recently proposed a series of novel corich twinning induced plasticity (TWIP) and transformation induced plasticity (TRIP) HEAs with superior tensile properties at room temperature; however, the hot deformation behavior has not been reported. Here, we investigated the dynamic recrystallization behavior and grain refinement of a representative TRIP-HEA, compressed at temperatures of 1123–1273 K with strain rates of 0.1–0.001 s<sup>−1</sup>. We characterized the impact of the temperature and strain rate on the grain structure evolution. A constitutive equation was constructed to reveal the correlations between the flow stress, strain rate, temperature, and strain. The apparent activation energy was estimated to be ~385.7 kJ/mol. The discontinuous dynamic recrystallization played an important role in the grain refinement, particularly at a relatively higher temperature and a lower strain rate, and the volume fraction and morphology of the recrystallized grains exhibited a strong dependency on the Zener–Hollomon parameter. The study provides guidelines for the grain refinement of HEAs through thermomechanical processing.https://www.mdpi.com/1996-1944/14/5/1196high-entropy alloyhot deformationdynamic recrystallizationconstitutive equationmicrostructure
spellingShingle Hailong Yi
Daixiu Wei
Renyi Xie
Yifan Zhang
Hidemi Kato
Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
Materials
high-entropy alloy
hot deformation
dynamic recrystallization
constitutive equation
microstructure
title Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
title_full Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
title_fullStr Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
title_full_unstemmed Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
title_short Microstructure Refinement of a Transformation-Induced Plasticity High-Entropy Alloy
title_sort microstructure refinement of a transformation induced plasticity high entropy alloy
topic high-entropy alloy
hot deformation
dynamic recrystallization
constitutive equation
microstructure
url https://www.mdpi.com/1996-1944/14/5/1196
work_keys_str_mv AT hailongyi microstructurerefinementofatransformationinducedplasticityhighentropyalloy
AT daixiuwei microstructurerefinementofatransformationinducedplasticityhighentropyalloy
AT renyixie microstructurerefinementofatransformationinducedplasticityhighentropyalloy
AT yifanzhang microstructurerefinementofatransformationinducedplasticityhighentropyalloy
AT hidemikato microstructurerefinementofatransformationinducedplasticityhighentropyalloy