Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions
Abstract Green synthesis of a noble metal such as Ag nanoparticles is an enormously developed research area. In this study, a biochar/Fe3O4–Ag magnetic nanocatalyst was produced via a green path by using Celery stalk as a carbon-based substrate and Celery leaf extract as reducing and stabilizing age...
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Format: | Article |
Language: | English |
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Nature Portfolio
2022-08-01
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Series: | Scientific Reports |
Online Access: | https://doi.org/10.1038/s41598-022-18131-w |
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author | Sahar Taheri Majid M. Heravi Pourya Mohammadi |
author_facet | Sahar Taheri Majid M. Heravi Pourya Mohammadi |
author_sort | Sahar Taheri |
collection | DOAJ |
description | Abstract Green synthesis of a noble metal such as Ag nanoparticles is an enormously developed research area. In this study, a biochar/Fe3O4–Ag magnetic nanocatalyst was produced via a green path by using Celery stalk as a carbon-based substrate and Celery leaf extract as reducing and stabilizing agents to construct Ag nanoparticles. The synthesized nanocatalyst was determined using various techniques, such as UV–Vis spectroscopy, FT-IR spectroscopy, XRD (X-ray diffraction), SEM/EDX spectroscopy (scanning electron microscopy/energy-dispersive X-ray), TEM (transmission electron microscopy), and VSM (vibrating sample magnetometer). To survey the catalytic action of the biochar/Fe3O4–Ag nanocatalyst, it was used in the reduction reaction of disparate nitroaromatics, aldehydes, and ketones. This catalyst has demonstrated good characteristics in terms of the amount, reusability, recoverability, activity, and structural integrity of the catalyst during the reaction. In addition, biochar/Fe3O4–Ag could be detached magnetically and recycled multiple times without significantly reducing its catalytic performance. |
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format | Article |
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institution | Directory Open Access Journal |
issn | 2045-2322 |
language | English |
last_indexed | 2024-04-11T22:36:02Z |
publishDate | 2022-08-01 |
publisher | Nature Portfolio |
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series | Scientific Reports |
spelling | doaj.art-b20a549c74534c49aa2dd054f05472de2022-12-22T03:59:13ZengNature PortfolioScientific Reports2045-23222022-08-0112111110.1038/s41598-022-18131-wSynthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactionsSahar Taheri0Majid M. Heravi1Pourya Mohammadi2Department of Chemistry, Faculty of Physics and Chemistry, Alzahra UniversityDepartment of Chemistry, Faculty of Physics and Chemistry, Alzahra UniversityDepartment of Chemistry, Faculty of Physics and Chemistry, Alzahra UniversityAbstract Green synthesis of a noble metal such as Ag nanoparticles is an enormously developed research area. In this study, a biochar/Fe3O4–Ag magnetic nanocatalyst was produced via a green path by using Celery stalk as a carbon-based substrate and Celery leaf extract as reducing and stabilizing agents to construct Ag nanoparticles. The synthesized nanocatalyst was determined using various techniques, such as UV–Vis spectroscopy, FT-IR spectroscopy, XRD (X-ray diffraction), SEM/EDX spectroscopy (scanning electron microscopy/energy-dispersive X-ray), TEM (transmission electron microscopy), and VSM (vibrating sample magnetometer). To survey the catalytic action of the biochar/Fe3O4–Ag nanocatalyst, it was used in the reduction reaction of disparate nitroaromatics, aldehydes, and ketones. This catalyst has demonstrated good characteristics in terms of the amount, reusability, recoverability, activity, and structural integrity of the catalyst during the reaction. In addition, biochar/Fe3O4–Ag could be detached magnetically and recycled multiple times without significantly reducing its catalytic performance.https://doi.org/10.1038/s41598-022-18131-w |
spellingShingle | Sahar Taheri Majid M. Heravi Pourya Mohammadi Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions Scientific Reports |
title | Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions |
title_full | Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions |
title_fullStr | Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions |
title_full_unstemmed | Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions |
title_short | Synthesis of Ag nanoparticles by Celery leaves extract supported on magnetic biochar substrate, as a catalyst for the reduction reactions |
title_sort | synthesis of ag nanoparticles by celery leaves extract supported on magnetic biochar substrate as a catalyst for the reduction reactions |
url | https://doi.org/10.1038/s41598-022-18131-w |
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