Effect of different precursors in the chemical synthesis of ZnO nanocrystals
This work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and T...
| Main Authors: | , , , , , , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)
2011-01-01
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| Series: | Materials Research |
| Subjects: | |
| Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020 |
| _version_ | 1811274834037964800 |
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| author | Marivone Gusatti Gilvan Sérgio Barroso Carlos Eduardo Maduro de Campos Daniel Aragão Ribeiro de Souza Jeane de Almeida do Rosário Raquel Bohn Lima Camila Cardoso Milioli Laura Abreu Silva Humberto Gracher Riella Nivaldo Cabral Kuhnen |
| author_facet | Marivone Gusatti Gilvan Sérgio Barroso Carlos Eduardo Maduro de Campos Daniel Aragão Ribeiro de Souza Jeane de Almeida do Rosário Raquel Bohn Lima Camila Cardoso Milioli Laura Abreu Silva Humberto Gracher Riella Nivaldo Cabral Kuhnen |
| author_sort | Marivone Gusatti |
| collection | DOAJ |
| description | This work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and TEM. The analysis have provided evidences that the material obtained applying Zn(NO3)2.6H2O as precursor has hexagonal crystalline structure, typical of the ZnO, and dimensions in the nanoscale. However, applying ZnCl2 as precursor results in a mixture of ZnO and Zn5(OH)8Cl2.H2O phases. For both precursors, the predominant morphology of the obtained ZnO nanocrystals was the rod-like structure. |
| first_indexed | 2024-04-12T23:27:20Z |
| format | Article |
| id | doaj.art-b29ca2c364c1478bbdebd1667a22c3d8 |
| institution | Directory Open Access Journal |
| issn | 1516-1439 |
| language | English |
| last_indexed | 2024-04-12T23:27:20Z |
| publishDate | 2011-01-01 |
| publisher | Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol) |
| record_format | Article |
| series | Materials Research |
| spelling | doaj.art-b29ca2c364c1478bbdebd1667a22c3d82022-12-22T03:12:23ZengAssociação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)Materials Research1516-14392011-01-01142264267Effect of different precursors in the chemical synthesis of ZnO nanocrystalsMarivone GusattiGilvan Sérgio BarrosoCarlos Eduardo Maduro de CamposDaniel Aragão Ribeiro de SouzaJeane de Almeida do RosárioRaquel Bohn LimaCamila Cardoso MilioliLaura Abreu SilvaHumberto Gracher RiellaNivaldo Cabral KuhnenThis work evaluates the effect of ZnCl2 and Zn(NO3)2.6H2O as precursors in the synthesis of ZnO nanocrystals. The materials were obtained at 90 ºC by a simple solochemical route. The resulting samples were characterized regarding phase composition, particle size and morphology, by means of XRD and TEM. The analysis have provided evidences that the material obtained applying Zn(NO3)2.6H2O as precursor has hexagonal crystalline structure, typical of the ZnO, and dimensions in the nanoscale. However, applying ZnCl2 as precursor results in a mixture of ZnO and Zn5(OH)8Cl2.H2O phases. For both precursors, the predominant morphology of the obtained ZnO nanocrystals was the rod-like structure.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020nanocrystalline materialszinc oxidesolochemical method |
| spellingShingle | Marivone Gusatti Gilvan Sérgio Barroso Carlos Eduardo Maduro de Campos Daniel Aragão Ribeiro de Souza Jeane de Almeida do Rosário Raquel Bohn Lima Camila Cardoso Milioli Laura Abreu Silva Humberto Gracher Riella Nivaldo Cabral Kuhnen Effect of different precursors in the chemical synthesis of ZnO nanocrystals Materials Research nanocrystalline materials zinc oxide solochemical method |
| title | Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
| title_full | Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
| title_fullStr | Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
| title_full_unstemmed | Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
| title_short | Effect of different precursors in the chemical synthesis of ZnO nanocrystals |
| title_sort | effect of different precursors in the chemical synthesis of zno nanocrystals |
| topic | nanocrystalline materials zinc oxide solochemical method |
| url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392011000200020 |
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