N′-(2-Hydroxy-3-methoxybenzylidene)pyrazine-2-carbohydrazide monohydrate

N′-(2-Hydroxy-3-methoxybenzylidene)pyrazine-2-carbohydrazide monohydrate

In the title hydrated Schiff base, C13H12N4O3·H2O, the dihedral angle between the aromatic rings is 5.06 (11)° and an intramolecular O—H...N hydrogen bond closes an S(6) ring. In the crystal, Ow—H...O and Ow—H...N (w = water) hydrogen bonds link the components into centrosymmetric tetramers (two Sch...

Full description

Bibliographic Details
Main Author:	Zhaodong Wang
Format:	Article
Language:	English
Published:	International Union of Crystallography 2020-01-01
Series:	IUCrData
Subjects:	crystal structure schiff base acylhydrazone ligand hydrogen bonding
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2414314619017310

Similar Items

Methyl 4-{N′-[(1E)-1-(pyrazin-2-yl)ethylidene]hydrazinecarbonyl}benzoate
by: Zhaodong Wang, et al.
Published: (2018-09-01)

N′-[1-(Pyrazin-2-yl)ethylidene]pyrazine-2-carbohydrazide
by: Zhaodong Wang
Published: (2018-08-01)

N,N′-Bis(pyrazin-2-ylmethyl)pyrazine-2,3-dicarboxamide
by: Zhaodong Wang, et al.
Published: (2016-10-01)

4,4′-Methylenebis[N-(2-hydroxy-3-methoxybenzylidene)-2,6-diisopropylaniline]
by: Tulasi Prapakaran, et al.
Published: (2022-08-01)

1-[(E)-(3-Hydroxy-4-methoxybenzylidene)amino]-3-methylthiourea
by: Md. Azharul Arafath, et al.
Published: (2016-10-01)

Crystal structure of ethyl 4-[(E)-(4-hydroxy-3-methoxybenzylidene)amino]benzoate: a p-hydroxy Schiff base
by: Jing Ling, et al.
Published: (2016-07-01)

Crystal structure and Hirshfeld surface analysis of (±)-N′-(2-hydroxy-3-methoxybenzylidene)-2-(4-isobutylphenyl)propionohydrazide
by: Shaaban K. Mohamed, et al.
Published: (2022-08-01)

N-(3-{[(Z)-(3-Hydroxy-4-methylphenyl)imino]methyl}pyridin-2-yl)pivalamide
by: Şehriman Atalay, et al.
Published: (2016-03-01)

Crystal structure of ethyl 2-(2-{(1E)-[(E)-2-(2-hydroxybenzylidene)hydrazin-1-ylidene]methyl}phenoxy)acetate
by: Mehmet Akkurt, et al.
Published: (2015-02-01)

(E)-4-Methoxy-N′-(2,4,5-trifluorobenzylidene)benzohydrazide monohydrate
by: R. Maheswari, et al.
Published: (2016-05-01)

N′-[(1E)-4-Hydroxy-3-methoxybenzylidene]isonicotinohydrazide monohydrate
by: K. R. Roopashree, et al.
Published: (2016-08-01)

2,4-Dibromo-6-[(2-hydroxy-5-methylanilino)methylidene]cyclohexa-2,4-dienone
by: Tarun Kumar Pal, et al.
Published: (2018-03-01)

2,4-Dichloro-6-[(2-hydroxy-5-methylanilino)methylidene]cyclohexa-2,4-dienone
by: Tarun Kumar Pal, et al.
Published: (2019-10-01)

Synthesis and characterization of four N-acylhydrazones as potential O,N,O donors for Cu2+: An experimental and theoretical study
by: María Mercedes Hincapié Otero, et al.
Published: (2021-07-01)

Crystal structure and Hirshfeld surface analysis of N,N′-bis(3-tert-butyl-2-hydroxy-5-methylbenzylidene)ethane-1,2-diamine
by: Pinar Sen, et al.
Published: (2018-08-01)

(E)-4-Bromo-5-methoxy-2-{[(2-methoxyphenyl)imino]methyl}phenol monohydrate
by: Şehriman Atalay, et al.
Published: (2017-12-01)

(E)-N-{3-[(m-Tolylimino)methyl]pyridin-2-yl}pivalamide
by: Şehriman Atalay, et al.
Published: (2017-11-01)

Crystal structure, Hirshfeld surface analysis and HOMO–LUMO analysis of (E)-N′-(3-hydroxy-4-methoxybenzylidene)nicotinohydrazide monohydrate
by: Palaniyappan Sivajeyanthi, et al.
Published: (2019-06-01)

Crystal structure of S-hexyl (E)-3-(2-hydroxybenzylidene)dithiocarbazate
by: M. S. Begum, et al.
Published: (2016-03-01)

(5-Hydroxy-3-methyl-5-trifluoromethyl-4,5-dihydro-1H-pyrazol-1-yl)(2-hydroxyphenyl)methanone
by: Kuvondik G. Avezov, et al.
Published: (2016-03-01)

6-[(2-Hydroxy-5-methylanilino)methylidene]-4-nitrocyclohexa-2,4-dien-1-one
by: Uwe Böhme, et al.
Published: (2020-10-01)

Crystal structure of (E)-N-[(2-methoxynaphthalen-1-yl)methylidene]-3-nitroaniline
by: Devika Bhai R., et al.
Published: (2015-12-01)

Crystal structure of 4-bromo-2-[(E)-N-(2,2,6,6-tetramethylpiperidin-4-yl)carboximidoyl]phenol dihydrate
by: Joel T. Mague, et al.
Published: (2015-05-01)

Crystal structure of 3-benzoyl-2-[(5-bromo-2-hydroxy-3-methoxybenzylidene)amino]-4,5,6,7-tetrahydrobenzo[b]thiophene
by: Manpreet Kaur, et al.
Published: (2015-02-01)

Crystal structure, Hirshfeld surface analysis and geometry optimization of 2-hydroxyimino-N-[1-(pyrazin-2-yl)ethylidene]propanohydrazide
by: Maksym O. Plutenko, et al.
Published: (2022-09-01)

(E)-2-{[(4-Anilinophenyl)imino]methyl}-4-bromo-5-fluorophenol
by: Sedanur Kalecik, et al.
Published: (2017-12-01)

Crystal structure of N-[3-(2-chlorobenzoyl)-5-ethylthiophen-2-yl]-2-[(E)-(2-hydroxybenzylidene)amino]acetamide
by: Manpreet Kaur, et al.
Published: (2014-09-01)

(E)-N′-Benzylidene-2-phenylquinoline-4-carbohydrazide
by: Joel T. Mague, et al.
Published: (2016-10-01)

Crystal structure and Hirshfeld surface analysis of (Z)-6-[(2-hydroxy-4-methylanilino)methylidene]-4-methylcyclohexa-2,4-dien-1-one
by: Sevgi Kansiz, et al.
Published: (2019-06-01)

Benzyl 3-(3,4,5-trimethoxybenzylidene)dithiocarbazate
by: M. A. A. A. A. Islam, et al.
Published: (2016-02-01)

Crystal structure of diethylammonium dioxido{Z)-N-[(pyridin-2-yl)carbonylazanidyl]pyridine-2-carboximidato}vanadate(1−) monohydrate
by: Bipul Mondal
Published: (2024-03-01)

N,N-Dimethyl-2-[(1E)-({[(methylsulfanyl)methanethioyl]amino}imino)methyl]aniline
by: Winaki P. Sohtun, et al.
Published: (2018-03-01)

Crystal structure of 2-hydroxy-N-(2-hydroxyethyl)-N-{2-hydroxy-3-[(E)-N-hydroxyethanimidoyl]-5-methylbenzyl}ethanaminium acetate monohydrate
by: Gary S. Nichol, et al.
Published: (2015-03-01)

N′-[(E)-4-Methoxybenzylidene]-2-(4-methylphenoxy)acetohydrazide
by: Seranthimata Samshuddin, et al.
Published: (2016-11-01)

Crystal structure of 1,2-bis((benzylsulfanyl){2-[1-(2-hydroxyphenyl)ethylidene]hydrazin-1-ylidene}methyl)disulfane
by: M. A. A. A. A. Islam, et al.
Published: (2016-03-01)

Crystal structure of 4-nitro-N-[(pyridin-2-yl)methylidene]aniline
by: Watcharin Saphu, et al.
Published: (2015-10-01)

(Z)-3-Allyl-5-(3-methoxybenzylidene)-2-sulfanylidene-1,3-thiazolidin-4-one
by: Rahhal El Ajlaoui, et al.
Published: (2016-01-01)

Chloridobis(ethane-1,2-diamine-κ2N,N′)(3-methylpyridine-κN)cobalt(III) dichloride monohydrate
by: K. Hemanathan, et al.
Published: (2018-07-01)

Crystal structure of (E)-5-benzyloxy-2-{[(4-nitrophenyl)imino]methyl}phenol
by: Nadir Ghichi, et al.
Published: (2015-12-01)

N-[(E)-Quinolin-2-ylmethylidene]-1,2,4-triazol-4-amine hemihydrate
by: Nurulizzatul Ningsheh M. Shahri, et al.
Published: (2020-02-01)