Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties
MoO3 thick film was manufactured by using a thermal spray process (Atmospheric Plasma Spray, or APS) and its microstructure, phase composition and properties of the coating layer were investigated. Initial powder feedstock was composed of an orthorhombic α-MoO3 phase, and the average powder particle...
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Polish Academy of Sciences
2022-11-01
|
| Series: | Archives of Metallurgy and Materials |
| Subjects: | |
| Online Access: | https://journals.pan.pl/Content/125129/PDF/AMM-2022-4-47-Kee-Ahn%20Lee.pdf |
| _version_ | 1828185946733936640 |
|---|---|
| author | Yu-Jin Hwang Kyu-Sik Kim Jae-Sung Park Kee-Ahn Lee |
| author_facet | Yu-Jin Hwang Kyu-Sik Kim Jae-Sung Park Kee-Ahn Lee |
| author_sort | Yu-Jin Hwang |
| collection | DOAJ |
| description | MoO3 thick film was manufactured by using a thermal spray process (Atmospheric Plasma Spray, or APS) and its microstructure, phase composition and properties of the coating layer were investigated. Initial powder feedstock was composed of an orthorhombic α-MoO3 phase, and the average powder particle size was 6.7 μm. As a result of the APS coating process, a MoO3 coating layer with a thickness of about 90 μm was obtained. Phase transformation occurred during the process, and the coating layer consisted of not only α-MoO3 but also β-MoO3, MoO2. Phase transformation could be due to the rapid cooling that occurred during the process. The properties of the coating layer were evaluated using a nano indentation test. Hardness and reduced modulus were obtained as 0.47 GPa and 1.4 GPa, respectively. Based on the above results, the possibility of manufacturing a MoO3 thick coating layer using thermal spray is presented. |
| first_indexed | 2024-04-12T07:11:57Z |
| format | Article |
| id | doaj.art-b32c842adc9143a2a0fe612564ea6ad9 |
| institution | Directory Open Access Journal |
| issn | 2300-1909 |
| language | English |
| last_indexed | 2024-04-12T07:11:57Z |
| publishDate | 2022-11-01 |
| publisher | Polish Academy of Sciences |
| record_format | Article |
| series | Archives of Metallurgy and Materials |
| spelling | doaj.art-b32c842adc9143a2a0fe612564ea6ad92022-12-22T03:42:37ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092022-11-01vol. 67No 415351538https://doi.org/10.24425/amm.2022.141089Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and PropertiesYu-Jin Hwang0https://orcid.org/0000-0002-7481-4088Kyu-Sik Kim1https://orcid.org/0000-0001-5649-8299Jae-Sung Park2Kee-Ahn Lee3https://orcid.org/0000-0003-2149-3871Inha University, Department of Materials Science and Engineering, Incheon, KoreaInha University, Department of Materials Science and Engineering, Incheon, KoreaLT Metal, Seoul, KoreaInha University, Department of Materials Science and Engineering, Incheon, KoreaMoO3 thick film was manufactured by using a thermal spray process (Atmospheric Plasma Spray, or APS) and its microstructure, phase composition and properties of the coating layer were investigated. Initial powder feedstock was composed of an orthorhombic α-MoO3 phase, and the average powder particle size was 6.7 μm. As a result of the APS coating process, a MoO3 coating layer with a thickness of about 90 μm was obtained. Phase transformation occurred during the process, and the coating layer consisted of not only α-MoO3 but also β-MoO3, MoO2. Phase transformation could be due to the rapid cooling that occurred during the process. The properties of the coating layer were evaluated using a nano indentation test. Hardness and reduced modulus were obtained as 0.47 GPa and 1.4 GPa, respectively. Based on the above results, the possibility of manufacturing a MoO3 thick coating layer using thermal spray is presented.https://journals.pan.pl/Content/125129/PDF/AMM-2022-4-47-Kee-Ahn%20Lee.pdfmoo3thermal sprayatmospheric plasma spraymicrostructureproperties |
| spellingShingle | Yu-Jin Hwang Kyu-Sik Kim Jae-Sung Park Kee-Ahn Lee Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties Archives of Metallurgy and Materials moo3 thermal spray atmospheric plasma spray microstructure properties |
| title | Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties |
| title_full | Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties |
| title_fullStr | Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties |
| title_full_unstemmed | Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties |
| title_short | Manufacture of MoO3 Coating Layer Using Thermal Spray Process and Analysis of Microstructure and Properties |
| title_sort | manufacture of moo3 coating layer using thermal spray process and analysis of microstructure and properties |
| topic | moo3 thermal spray atmospheric plasma spray microstructure properties |
| url | https://journals.pan.pl/Content/125129/PDF/AMM-2022-4-47-Kee-Ahn%20Lee.pdf |
| work_keys_str_mv | AT yujinhwang manufactureofmoo3coatinglayerusingthermalsprayprocessandanalysisofmicrostructureandproperties AT kyusikkim manufactureofmoo3coatinglayerusingthermalsprayprocessandanalysisofmicrostructureandproperties AT jaesungpark manufactureofmoo3coatinglayerusingthermalsprayprocessandanalysisofmicrostructureandproperties AT keeahnlee manufactureofmoo3coatinglayerusingthermalsprayprocessandanalysisofmicrostructureandproperties |