Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质)
采用AS19离子色谱分析柱和KOH梯度淋洗,用抑制电导检测器对甘油磷酸钠注射液中主要成分以及氟离子、氯离子、磷酸根等杂质阴离子同时进行检测,被测物质甘油磷酸根的保留时间和峰面积的相对标准差分别小于0.339%和2.617%；被测物质的线性相关系数为0.999 7~1.000 0；加标回收率为90.5%~103%.采用该方法对实际样品的检测,结果令人满意....
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| Format: | Article |
| Language: | zho |
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Zhejiang University Press
2009-01-01
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| Series: | Zhejiang Daxue xuebao. Lixue ban |
| Subjects: | |
| Online Access: | https://doi.org/10.3785/j.issn.1008-9497.2009.01.016 |
| _version_ | 1797236174129987584 |
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| author | YAOChao-ying(姚超英) |
| author_facet | YAOChao-ying(姚超英) |
| author_sort | YAOChao-ying(姚超英) |
| collection | DOAJ |
| description | 采用AS19离子色谱分析柱和KOH梯度淋洗,用抑制电导检测器对甘油磷酸钠注射液中主要成分以及氟离子、氯离子、磷酸根等杂质阴离子同时进行检测,被测物质甘油磷酸根的保留时间和峰面积的相对标准差分别小于0.339%和2.617%；被测物质的线性相关系数为0.999 7~1.000 0；加标回收率为90.5%~103%.采用该方法对实际样品的检测,结果令人满意. |
| first_indexed | 2024-04-24T16:59:39Z |
| format | Article |
| id | doaj.art-b37e2e298fa2465ba8d324c7b0e0170b |
| institution | Directory Open Access Journal |
| issn | 1008-9497 |
| language | zho |
| last_indexed | 2024-04-24T16:59:39Z |
| publishDate | 2009-01-01 |
| publisher | Zhejiang University Press |
| record_format | Article |
| series | Zhejiang Daxue xuebao. Lixue ban |
| spelling | doaj.art-b37e2e298fa2465ba8d324c7b0e0170b2024-03-29T01:58:26ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972009-01-01361777910.3785/j.issn.1008-9497.2009.01.016Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质)YAOChao-ying(姚超英)0 1.Department of Chemical Engineering, Hangzhou Vocational and Technical College, Hangzhou 310018, China( 1.杭州职业技术学院化工系，浙江 杭州 310018)采用AS19离子色谱分析柱和KOH梯度淋洗,用抑制电导检测器对甘油磷酸钠注射液中主要成分以及氟离子、氯离子、磷酸根等杂质阴离子同时进行检测,被测物质甘油磷酸根的保留时间和峰面积的相对标准差分别小于0.339%和2.617%；被测物质的线性相关系数为0.999 7~1.000 0；加标回收率为90.5%~103%.采用该方法对实际样品的检测,结果令人满意.https://doi.org/10.3785/j.issn.1008-9497.2009.01.016离子色谱梯度淋洗甘油磷酸钠杂质阴离子 |
| spellingShingle | YAOChao-ying(姚超英) Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) Zhejiang Daxue xuebao. Lixue ban 离子色谱 梯度淋洗 甘油磷酸钠 杂质阴离子 |
| title | Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) |
| title_full | Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) |
| title_fullStr | Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) |
| title_full_unstemmed | Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) |
| title_short | Determination of component and impurity in sodium glycerophospate injection by ion chromatography(离子色谱法测定甘油磷酸钠注射液的成分及杂质) |
| title_sort | determination of component and impurity in sodium glycerophospate injection by ion chromatography 离子色谱法测定甘油磷酸钠注射液的成分及杂质 |
| topic | 离子色谱 梯度淋洗 甘油磷酸钠 杂质阴离子 |
| url | https://doi.org/10.3785/j.issn.1008-9497.2009.01.016 |
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