The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate
A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic...
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| Format: | Article |
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MDPI AG
2013-05-01
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| Series: | Crystals |
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| Online Access: | http://www.mdpi.com/2073-4352/3/2/333 |
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| author | Andreas Decken Christopher M. Vogels L. Ross C. Barclay Kate J. Sullivan Dylan T. McLaughlin Raymond Roy Steven R. Hall Stephen A. Westcott |
| author_facet | Andreas Decken Christopher M. Vogels L. Ross C. Barclay Kate J. Sullivan Dylan T. McLaughlin Raymond Roy Steven R. Hall Stephen A. Westcott |
| author_sort | Andreas Decken |
| collection | DOAJ |
| description | A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules. |
| first_indexed | 2024-04-14T01:51:53Z |
| format | Article |
| id | doaj.art-b3f63ede10c24950988848be86fa87c2 |
| institution | Directory Open Access Journal |
| issn | 2073-4352 |
| language | English |
| last_indexed | 2024-04-14T01:51:53Z |
| publishDate | 2013-05-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Crystals |
| spelling | doaj.art-b3f63ede10c24950988848be86fa87c22022-12-22T02:19:20ZengMDPI AGCrystals2073-43522013-05-013233333810.3390/cryst3020333The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol SolvateAndreas DeckenChristopher M. VogelsL. Ross C. BarclayKate J. SullivanDylan T. McLaughlinRaymond RoySteven R. HallStephen A. WestcottA 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.http://www.mdpi.com/2073-4352/3/2/333dopaminehydroxypyridinoneligandX-ray |
| spellingShingle | Andreas Decken Christopher M. Vogels L. Ross C. Barclay Kate J. Sullivan Dylan T. McLaughlin Raymond Roy Steven R. Hall Stephen A. Westcott The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate Crystals dopamine hydroxypyridinone ligand X-ray |
| title | The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate |
| title_full | The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate |
| title_fullStr | The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate |
| title_full_unstemmed | The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate |
| title_short | The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate |
| title_sort | synthesis and molecular structure of 1 3 4 dihydroxyphenethyl 3 hydroxy 2 methylpyridin 4 1h one hydrochloride methanol solvate |
| topic | dopamine hydroxypyridinone ligand X-ray |
| url | http://www.mdpi.com/2073-4352/3/2/333 |
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