Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
Solid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an at...
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MDPI AG
2023-09-01
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Series: | Molecules |
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Online Access: | https://www.mdpi.com/1420-3049/28/19/6880 |
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author | Snezana Agatonovic-Kustrin Vladimir Gegechkori Tamara Kobakhidze David Morton |
author_facet | Snezana Agatonovic-Kustrin Vladimir Gegechkori Tamara Kobakhidze David Morton |
author_sort | Snezana Agatonovic-Kustrin |
collection | DOAJ |
description | Solid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an attractive choice for many analytical applications. SPME has been widely applied to the sampling and analysis of environmental, food, aromatic, metallic, forensic, and pharmaceutical samples. Solid phase microextraction is used in horticultural crops, for example, to determine water and soil contaminants (pesticides, alcohols, phenols, amines, herbicides, etc.). SPME is also used in the food industry to separate biologically active substances in food products for various purposes, for example, disease prevention, determining the smell of food products, and analyzing tastes. SPME has been applied to forensic analysis to determine the alcohol concentration in blood and that of sugar in urine. This method has also been widely used in pharmaceutical analysis. It is a solvent-free sample preparation technique that integrates sampling, isolation, and concentration. This review focuses on recent work on the use of SPME techniques in the analysis of food and horticultural crops. |
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language | English |
last_indexed | 2024-03-10T21:40:06Z |
publishDate | 2023-09-01 |
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series | Molecules |
spelling | doaj.art-b6388113c49144b19b846594b196cbe42023-11-19T14:46:50ZengMDPI AGMolecules1420-30492023-09-012819688010.3390/molecules28196880Solid-Phase Microextraction Techniques and Application in Food and Horticultural CropsSnezana Agatonovic-Kustrin0Vladimir Gegechkori1Tamara Kobakhidze2David Morton3Department of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaSolid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an attractive choice for many analytical applications. SPME has been widely applied to the sampling and analysis of environmental, food, aromatic, metallic, forensic, and pharmaceutical samples. Solid phase microextraction is used in horticultural crops, for example, to determine water and soil contaminants (pesticides, alcohols, phenols, amines, herbicides, etc.). SPME is also used in the food industry to separate biologically active substances in food products for various purposes, for example, disease prevention, determining the smell of food products, and analyzing tastes. SPME has been applied to forensic analysis to determine the alcohol concentration in blood and that of sugar in urine. This method has also been widely used in pharmaceutical analysis. It is a solvent-free sample preparation technique that integrates sampling, isolation, and concentration. This review focuses on recent work on the use of SPME techniques in the analysis of food and horticultural crops.https://www.mdpi.com/1420-3049/28/19/6880foodshead space extractiongas chromatography–mass spectroscopypesticidesfoodssolid phase microextraction |
spellingShingle | Snezana Agatonovic-Kustrin Vladimir Gegechkori Tamara Kobakhidze David Morton Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops Molecules foods head space extraction gas chromatography–mass spectroscopy pesticides foods solid phase microextraction |
title | Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops |
title_full | Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops |
title_fullStr | Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops |
title_full_unstemmed | Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops |
title_short | Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops |
title_sort | solid phase microextraction techniques and application in food and horticultural crops |
topic | foods head space extraction gas chromatography–mass spectroscopy pesticides foods solid phase microextraction |
url | https://www.mdpi.com/1420-3049/28/19/6880 |
work_keys_str_mv | AT snezanaagatonovickustrin solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops AT vladimirgegechkori solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops AT tamarakobakhidze solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops AT davidmorton solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops |