Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops

Solid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an at...

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Main Authors: Snezana Agatonovic-Kustrin, Vladimir Gegechkori, Tamara Kobakhidze, David Morton
Format: Article
Language:English
Published: MDPI AG 2023-09-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/28/19/6880
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author Snezana Agatonovic-Kustrin
Vladimir Gegechkori
Tamara Kobakhidze
David Morton
author_facet Snezana Agatonovic-Kustrin
Vladimir Gegechkori
Tamara Kobakhidze
David Morton
author_sort Snezana Agatonovic-Kustrin
collection DOAJ
description Solid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an attractive choice for many analytical applications. SPME has been widely applied to the sampling and analysis of environmental, food, aromatic, metallic, forensic, and pharmaceutical samples. Solid phase microextraction is used in horticultural crops, for example, to determine water and soil contaminants (pesticides, alcohols, phenols, amines, herbicides, etc.). SPME is also used in the food industry to separate biologically active substances in food products for various purposes, for example, disease prevention, determining the smell of food products, and analyzing tastes. SPME has been applied to forensic analysis to determine the alcohol concentration in blood and that of sugar in urine. This method has also been widely used in pharmaceutical analysis. It is a solvent-free sample preparation technique that integrates sampling, isolation, and concentration. This review focuses on recent work on the use of SPME techniques in the analysis of food and horticultural crops.
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spelling doaj.art-b6388113c49144b19b846594b196cbe42023-11-19T14:46:50ZengMDPI AGMolecules1420-30492023-09-012819688010.3390/molecules28196880Solid-Phase Microextraction Techniques and Application in Food and Horticultural CropsSnezana Agatonovic-Kustrin0Vladimir Gegechkori1Tamara Kobakhidze2David Morton3Department of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaDepartment of Pharmaceutical and Toxicological Chemistry Named after Arzamastsev of the Institute of Pharmacy, I.M. Sechenov First Moscow State Medical University (Sechenov University), 119991 Moscow, RussiaSolid-phase microextraction (SPME) is a sample preparation technique which utilizes small amounts of an extraction phase for the extraction of target analytes from investigated sample matrices. Its simplicity of use, relatively short sample processing time, and fiber reusability have made SPME an attractive choice for many analytical applications. SPME has been widely applied to the sampling and analysis of environmental, food, aromatic, metallic, forensic, and pharmaceutical samples. Solid phase microextraction is used in horticultural crops, for example, to determine water and soil contaminants (pesticides, alcohols, phenols, amines, herbicides, etc.). SPME is also used in the food industry to separate biologically active substances in food products for various purposes, for example, disease prevention, determining the smell of food products, and analyzing tastes. SPME has been applied to forensic analysis to determine the alcohol concentration in blood and that of sugar in urine. This method has also been widely used in pharmaceutical analysis. It is a solvent-free sample preparation technique that integrates sampling, isolation, and concentration. This review focuses on recent work on the use of SPME techniques in the analysis of food and horticultural crops.https://www.mdpi.com/1420-3049/28/19/6880foodshead space extractiongas chromatography–mass spectroscopypesticidesfoodssolid phase microextraction
spellingShingle Snezana Agatonovic-Kustrin
Vladimir Gegechkori
Tamara Kobakhidze
David Morton
Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
Molecules
foods
head space extraction
gas chromatography–mass spectroscopy
pesticides
foods
solid phase microextraction
title Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
title_full Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
title_fullStr Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
title_full_unstemmed Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
title_short Solid-Phase Microextraction Techniques and Application in Food and Horticultural Crops
title_sort solid phase microextraction techniques and application in food and horticultural crops
topic foods
head space extraction
gas chromatography–mass spectroscopy
pesticides
foods
solid phase microextraction
url https://www.mdpi.com/1420-3049/28/19/6880
work_keys_str_mv AT snezanaagatonovickustrin solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops
AT vladimirgegechkori solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops
AT tamarakobakhidze solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops
AT davidmorton solidphasemicroextractiontechniquesandapplicationinfoodandhorticulturalcrops