Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements

The low bond strength of lithium disilicate (LD) ceramics to dental resin cements remains a critical issue for dental applications because it leads to frequent replacement and causes tooth tissue destruction and consumption. The objective of this study was to examine the effects of atmospheric non-t...

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Main Authors: Yixuan Liao, Stephen J. Lombardo, Qingsong Yu
Format: Article
Language:English
Published: MDPI AG 2023-07-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/15/5376
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author Yixuan Liao
Stephen J. Lombardo
Qingsong Yu
author_facet Yixuan Liao
Stephen J. Lombardo
Qingsong Yu
author_sort Yixuan Liao
collection DOAJ
description The low bond strength of lithium disilicate (LD) ceramics to dental resin cements remains a critical issue for dental applications because it leads to frequent replacement and causes tooth tissue destruction and consumption. The objective of this study was to examine the effects of atmospheric non-thermal argon plasma (NTP) treatment on LD to improve its micro-shear bond strength (μSBS) with dental resin cements because LD mostly experiences shear stress for its commonly used dental applications as crowns or veneers. Argon plasma treatment was performed on hydrofluoric (HF) acid-etched LD surfaces, and then commercial resin cements were subsequently applied to the treated LD surfaces. The plasma treatment significantly reduced the water contact angle of the LD surface to less than 10° without changing the surface morphology. The μSBS test was performed with cement-bonded LD samples after 24 h and 30 days, as well as after 1000 cycles of thermal cycling. The test results show that, as compared with the untreated controls, 300 s of plasma treatment significantly improved the LD-resin cement bond strength by 59.1%. After 30 days of storage in DI water and 1000 cycles of thermal cycling, the plasma-treated LD samples show 84.2% and 44.8% higher bond strengths as compared to the control samples, respectively. The plasma treatment effect on LD surfaces diminished rapidly as the bond strength decreased to 25.5 MPa after aging in the air for 1 day prior to primer and cement application, suggesting that primers should be applied to the LD surfaces immediately after the plasma treatment. These results demonstrate that, when applied with caution, plasma treatment can activate LD surfaces and significantly improve the SBS of LD with dental resin cements in both short-term and long-term periods.
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spelling doaj.art-b66cba4d5f8a4b2aae4930247125b8322023-11-18T23:12:29ZengMDPI AGMaterials1996-19442023-07-011615537610.3390/ma16155376Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin CementsYixuan Liao0Stephen J. Lombardo1Qingsong Yu2Department of Mechanical and Aerospace Engineering, University of Missouri, E3411 Lafferre Hall, Columbia, MO 65211, USADepartment of Mechanical and Aerospace Engineering, University of Missouri, E3411 Lafferre Hall, Columbia, MO 65211, USADepartment of Mechanical and Aerospace Engineering, University of Missouri, E3411 Lafferre Hall, Columbia, MO 65211, USAThe low bond strength of lithium disilicate (LD) ceramics to dental resin cements remains a critical issue for dental applications because it leads to frequent replacement and causes tooth tissue destruction and consumption. The objective of this study was to examine the effects of atmospheric non-thermal argon plasma (NTP) treatment on LD to improve its micro-shear bond strength (μSBS) with dental resin cements because LD mostly experiences shear stress for its commonly used dental applications as crowns or veneers. Argon plasma treatment was performed on hydrofluoric (HF) acid-etched LD surfaces, and then commercial resin cements were subsequently applied to the treated LD surfaces. The plasma treatment significantly reduced the water contact angle of the LD surface to less than 10° without changing the surface morphology. The μSBS test was performed with cement-bonded LD samples after 24 h and 30 days, as well as after 1000 cycles of thermal cycling. The test results show that, as compared with the untreated controls, 300 s of plasma treatment significantly improved the LD-resin cement bond strength by 59.1%. After 30 days of storage in DI water and 1000 cycles of thermal cycling, the plasma-treated LD samples show 84.2% and 44.8% higher bond strengths as compared to the control samples, respectively. The plasma treatment effect on LD surfaces diminished rapidly as the bond strength decreased to 25.5 MPa after aging in the air for 1 day prior to primer and cement application, suggesting that primers should be applied to the LD surfaces immediately after the plasma treatment. These results demonstrate that, when applied with caution, plasma treatment can activate LD surfaces and significantly improve the SBS of LD with dental resin cements in both short-term and long-term periods.https://www.mdpi.com/1996-1944/16/15/5376lithium disilicateplasma treatmentmicro-shear bond strengthsurface treatmentdental resin cements
spellingShingle Yixuan Liao
Stephen J. Lombardo
Qingsong Yu
Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
Materials
lithium disilicate
plasma treatment
micro-shear bond strength
surface treatment
dental resin cements
title Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
title_full Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
title_fullStr Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
title_full_unstemmed Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
title_short Argon Plasma Treatment Effects on the Micro-Shear Bond Strength of Lithium Disilicate with Dental Resin Cements
title_sort argon plasma treatment effects on the micro shear bond strength of lithium disilicate with dental resin cements
topic lithium disilicate
plasma treatment
micro-shear bond strength
surface treatment
dental resin cements
url https://www.mdpi.com/1996-1944/16/15/5376
work_keys_str_mv AT yixuanliao argonplasmatreatmenteffectsonthemicroshearbondstrengthoflithiumdisilicatewithdentalresincements
AT stephenjlombardo argonplasmatreatmenteffectsonthemicroshearbondstrengthoflithiumdisilicatewithdentalresincements
AT qingsongyu argonplasmatreatmenteffectsonthemicroshearbondstrengthoflithiumdisilicatewithdentalresincements