Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy

The addition of Sn improves the properties of Mg–Bi-based alloys, and can potentially overcome the high-temperature limitations of magnesium (Mg) alloys. However, high-Sn alloying leads to stress concentration during hot extrusion. Hence, in this study, the dynamic recrystallization (DRX) mechanism...

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Main Authors: Guo-lei Liu, Wei-li Cheng, Lin Luo, Hui Yu, Li-fei Wang, Hang Li, Hong-xia Wang, Jin-hui Wang
Format: Article
Language:English
Published: Elsevier 2023-07-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785423012310
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author Guo-lei Liu
Wei-li Cheng
Lin Luo
Hui Yu
Li-fei Wang
Hang Li
Hong-xia Wang
Jin-hui Wang
author_facet Guo-lei Liu
Wei-li Cheng
Lin Luo
Hui Yu
Li-fei Wang
Hang Li
Hong-xia Wang
Jin-hui Wang
author_sort Guo-lei Liu
collection DOAJ
description The addition of Sn improves the properties of Mg–Bi-based alloys, and can potentially overcome the high-temperature limitations of magnesium (Mg) alloys. However, high-Sn alloying leads to stress concentration during hot extrusion. Hence, in this study, the dynamic recrystallization (DRX) mechanism and hot-deformation behavior of a novel precipitate-free Mg–0.25Bi–0.25Sn alloy during hot compression conducted at 250–400 °C with strain rate of 0.001–1 s−1 were examined in detail by constructing processing maps and deriving constitutive equation. The obtained correlation coefficient was 0.99113, indicating that the proposed method can adequately predict the hot deformation behavior of the studied alloy. The calculated average activation energy was 143.0336 kJ/mol. According to the processing maps, the ideal processing areas corresponded to the conditions of 300–400 °C/0.001 s−1/1 s−1 and 400 °C/0.1 s−1. In addition, a transformation of prismatic <a> slip to pyramidal II <c+a> slip was observed at 350 °C, and the continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) processes occurred during hot compression. The classification of the dominant DRX mechanisms was based on the Zener–Hollomon parameter (Z). Under high-Z deformation conditions, CDRX and DDRX occurred simultaneously; however, CDRX was the predominant process. Under medium-Z deformation conditions, DDRX was the only DRX process. Under low-Z deformation conditions, DDRX dominated over the DRX mechanism and was partially accompanied by CDRX.
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spelling doaj.art-b764693f39464d76a67cb92e962d88bb2023-08-11T05:33:07ZengElsevierJournal of Materials Research and Technology2238-78542023-07-0125497510Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloyGuo-lei Liu0Wei-li Cheng1Lin Luo2Hui Yu3Li-fei Wang4Hang Li5Hong-xia Wang6Jin-hui Wang7School of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaSchool of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China; Corresponding author.School of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaSchool of Materials Science and Engineering, Hebei University of Technology, Tianjin 300132, ChinaSchool of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaSchool of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaSchool of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaQinghai Provincial Key Laboratory of New Light Alloys, Qinghai Provincial Engineering Research Center of High Performance Light Metal Alloys and Forming, Qinghai University, Xining 810016, ChinaThe addition of Sn improves the properties of Mg–Bi-based alloys, and can potentially overcome the high-temperature limitations of magnesium (Mg) alloys. However, high-Sn alloying leads to stress concentration during hot extrusion. Hence, in this study, the dynamic recrystallization (DRX) mechanism and hot-deformation behavior of a novel precipitate-free Mg–0.25Bi–0.25Sn alloy during hot compression conducted at 250–400 °C with strain rate of 0.001–1 s−1 were examined in detail by constructing processing maps and deriving constitutive equation. The obtained correlation coefficient was 0.99113, indicating that the proposed method can adequately predict the hot deformation behavior of the studied alloy. The calculated average activation energy was 143.0336 kJ/mol. According to the processing maps, the ideal processing areas corresponded to the conditions of 300–400 °C/0.001 s−1/1 s−1 and 400 °C/0.1 s−1. In addition, a transformation of prismatic <a> slip to pyramidal II <c+a> slip was observed at 350 °C, and the continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) processes occurred during hot compression. The classification of the dominant DRX mechanisms was based on the Zener–Hollomon parameter (Z). Under high-Z deformation conditions, CDRX and DDRX occurred simultaneously; however, CDRX was the predominant process. Under medium-Z deformation conditions, DDRX was the only DRX process. Under low-Z deformation conditions, DDRX dominated over the DRX mechanism and was partially accompanied by CDRX.http://www.sciencedirect.com/science/article/pii/S2238785423012310Dilute Mg alloyHot compressionProcessing mapConstitutive equationDynamic recrystallization
spellingShingle Guo-lei Liu
Wei-li Cheng
Lin Luo
Hui Yu
Li-fei Wang
Hang Li
Hong-xia Wang
Jin-hui Wang
Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
Journal of Materials Research and Technology
Dilute Mg alloy
Hot compression
Processing map
Constitutive equation
Dynamic recrystallization
title Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
title_full Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
title_fullStr Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
title_full_unstemmed Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
title_short Hot compression deformation behavior and dynamic recrystallization of a precipitate-free Mg–Bi–Sn alloy
title_sort hot compression deformation behavior and dynamic recrystallization of a precipitate free mg bi sn alloy
topic Dilute Mg alloy
Hot compression
Processing map
Constitutive equation
Dynamic recrystallization
url http://www.sciencedirect.com/science/article/pii/S2238785423012310
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