Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace

Despite the environmental concerns raised every year by the generation of high volumes of wet olive pomace, it contains valuable phenolic compounds that are essential for the valorization of this by-product. In this work, an integrated process to recover phenolic compounds from wet olive pomace is p...

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Main Authors: Carmen M. Sánchez-Arévalo, Ane Pérez García-Serrano, María Cinta Vincent-Vela, Silvia Álvarez-Blanco
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Membranes
Subjects:
Online Access:https://www.mdpi.com/2077-0375/13/2/119
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author Carmen M. Sánchez-Arévalo
Ane Pérez García-Serrano
María Cinta Vincent-Vela
Silvia Álvarez-Blanco
author_facet Carmen M. Sánchez-Arévalo
Ane Pérez García-Serrano
María Cinta Vincent-Vela
Silvia Álvarez-Blanco
author_sort Carmen M. Sánchez-Arévalo
collection DOAJ
description Despite the environmental concerns raised every year by the generation of high volumes of wet olive pomace, it contains valuable phenolic compounds that are essential for the valorization of this by-product. In this work, an integrated process to recover phenolic compounds from wet olive pomace is proposed. It consists of ultrasound-assisted solid-liquid extraction, followed by ultrafiltration and nanofiltration. Several commercial membranes were studied at different operational conditions. The ultrafiltration stage allowed the purification of biophenols, which were obtained in the permeate stream. Regarding organic matter, satisfactory rejection values were obtained with both commercial UH030 and UP005 membranes (Microdyn Nadir), but the latter provided more efficient purification and higher values of permeate flux, above 18 L·h<sup>−1</sup>·m<sup>−2</sup> at 2.5 bar and 1.5 m·s<sup>−1</sup>. Later, this permeate stream was concentrated by means of a nanofiltration process, obtaining polyphenol rejection values that surpassed 85% with the commercial NF270 membrane (DuPont), then achieving the concentration of the previously purified polyphenols.
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spelling doaj.art-b77042cb0bcc4ec1afc16bc299cca7852023-11-16T22:01:37ZengMDPI AGMembranes2077-03752023-01-0113211910.3390/membranes13020119Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive PomaceCarmen M. Sánchez-Arévalo0Ane Pérez García-Serrano1María Cinta Vincent-Vela2Silvia Álvarez-Blanco3Research Institute for Industrial, Radiophysical and Environmental Safety (ISIRYM), Universitat Politècnica de València, Camino de Vera, s/n, 46022 Valencia, SpainResearch Institute for Industrial, Radiophysical and Environmental Safety (ISIRYM), Universitat Politècnica de València, Camino de Vera, s/n, 46022 Valencia, SpainResearch Institute for Industrial, Radiophysical and Environmental Safety (ISIRYM), Universitat Politècnica de València, Camino de Vera, s/n, 46022 Valencia, SpainResearch Institute for Industrial, Radiophysical and Environmental Safety (ISIRYM), Universitat Politècnica de València, Camino de Vera, s/n, 46022 Valencia, SpainDespite the environmental concerns raised every year by the generation of high volumes of wet olive pomace, it contains valuable phenolic compounds that are essential for the valorization of this by-product. In this work, an integrated process to recover phenolic compounds from wet olive pomace is proposed. It consists of ultrasound-assisted solid-liquid extraction, followed by ultrafiltration and nanofiltration. Several commercial membranes were studied at different operational conditions. The ultrafiltration stage allowed the purification of biophenols, which were obtained in the permeate stream. Regarding organic matter, satisfactory rejection values were obtained with both commercial UH030 and UP005 membranes (Microdyn Nadir), but the latter provided more efficient purification and higher values of permeate flux, above 18 L·h<sup>−1</sup>·m<sup>−2</sup> at 2.5 bar and 1.5 m·s<sup>−1</sup>. Later, this permeate stream was concentrated by means of a nanofiltration process, obtaining polyphenol rejection values that surpassed 85% with the commercial NF270 membrane (DuPont), then achieving the concentration of the previously purified polyphenols.https://www.mdpi.com/2077-0375/13/2/119ultrafiltrationnanofiltrationphenolic compoundswet olive pomaceintegrated processrejection
spellingShingle Carmen M. Sánchez-Arévalo
Ane Pérez García-Serrano
María Cinta Vincent-Vela
Silvia Álvarez-Blanco
Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
Membranes
ultrafiltration
nanofiltration
phenolic compounds
wet olive pomace
integrated process
rejection
title Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
title_full Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
title_fullStr Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
title_full_unstemmed Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
title_short Combining Ultrafiltration and Nanofiltration to Obtain a Concentrated Extract of Purified Polyphenols from Wet Olive Pomace
title_sort combining ultrafiltration and nanofiltration to obtain a concentrated extract of purified polyphenols from wet olive pomace
topic ultrafiltration
nanofiltration
phenolic compounds
wet olive pomace
integrated process
rejection
url https://www.mdpi.com/2077-0375/13/2/119
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