Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter

Aluminum metal matrix composites (Al MMCs) are a class of materials characterized by being light in weight and high hardness. Due to these properties, Al MMCs have various applications in the automobile, aeronautical and marine industries. Ceramic-reinforced Al MMCs in the form of sinters are known...

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Main Authors: Paweł Szymański, Paweł Popielarski, Dorota Czarnecka-Komorowska, Robert Sika, Katarzyna Gawdzińska
Format: Article
Language:English
Published: MDPI AG 2023-09-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/18/6106
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author Paweł Szymański
Paweł Popielarski
Dorota Czarnecka-Komorowska
Robert Sika
Katarzyna Gawdzińska
author_facet Paweł Szymański
Paweł Popielarski
Dorota Czarnecka-Komorowska
Robert Sika
Katarzyna Gawdzińska
author_sort Paweł Szymański
collection DOAJ
description Aluminum metal matrix composites (Al MMCs) are a class of materials characterized by being light in weight and high hardness. Due to these properties, Al MMCs have various applications in the automobile, aeronautical and marine industries. Ceramic-reinforced Al MMCs in the form of sinters are known for having excellent abrasive properties, which makes them an attractive material in certain fields of technology. The biggest problem in their production process is their low ability to infiltrate ceramics with alloys and consequently the difficulty of filling a ceramic preform. The castability of such composites has not yet been researched in detail. The aim of this study was to create aluminum metal matrix composite castings based on aluminum alloys (AlSi11) reinforced with an Al<sub>2</sub>O<sub>3</sub> sinter preform using a Castability Trials spiral mold, and then to determine the degree of saturation with the liquid metal of the produced ceramic shaped body (Castability Trials spiral). For the selected AlSi11 alloy, the liquidus (Tl) and solidus (Ts) temperatures were determined by performing thermal-derivation analysis during cooling, which is Tl—579.3 °C and Ts—573.9 °C. The resultant pressure necessary for the infiltration process was estimated for the reinforcement capillaries with the following dimensions: 10, 15, 20, 25, 30 and 35 microns. The following values were used to determine the capillary pressure (Pk): surface tension of the alloy—σ = 840 mN/m; the extreme wetting angle of the reinforcement by the metal—θ = 136°. It has been experimentally confirmed that for the vacuum saturation process, the estimated resultant pressure enables saturation of reinforcement with capillaries larger than 25 microns, provided that the alloy temperature does not drop lower than the infiltration temperature. After the experiment, the time and route of the liquid metal flow in the spiral were determined. On the basis of the obtained values, a simulation was developed and initial assumptions such as saturation time, alloy temperature, reinforcement and mold temperature were verified. The energy balance showed that the saturation limit temperature was Tk = 580.7 °C for the reinforcement temperature of 575 °C. In contrast to the above, the assumption that the temperature of the metal after equalizing the temperature of the composite components must be higher than the liquidus temperature (Tliq = 579.3 °C) for the aluminum alloy used must be fulfilled. After the experiment, the time and path of the liquid metal flow in the spiral were determined. Then, on the basis of the obtained values, a simulation was developed, and the initial assumptions (saturation time and temperature) were verified.
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spelling doaj.art-b8220a9e3f154bb08b9e9e7e55c23f8b2023-11-19T11:43:02ZengMDPI AGMaterials1996-19442023-09-011618610610.3390/ma16186106Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> SinterPaweł Szymański0Paweł Popielarski1Dorota Czarnecka-Komorowska2Robert Sika3Katarzyna Gawdzińska4Institute of Materials Technology, Poznan University of Technology, Piotrowo 3 Str., 61-138 Poznan, PolandInstitute of Materials Technology, Poznan University of Technology, Piotrowo 3 Str., 61-138 Poznan, PolandInstitute of Materials Technology, Poznan University of Technology, Piotrowo 3 Str., 61-138 Poznan, PolandInstitute of Materials Technology, Poznan University of Technology, Piotrowo 3 Str., 61-138 Poznan, PolandFaculty of Marine Engineering, Maritime University of Szczecin, Willowa 2-4, 71-650 Szczecin, PolandAluminum metal matrix composites (Al MMCs) are a class of materials characterized by being light in weight and high hardness. Due to these properties, Al MMCs have various applications in the automobile, aeronautical and marine industries. Ceramic-reinforced Al MMCs in the form of sinters are known for having excellent abrasive properties, which makes them an attractive material in certain fields of technology. The biggest problem in their production process is their low ability to infiltrate ceramics with alloys and consequently the difficulty of filling a ceramic preform. The castability of such composites has not yet been researched in detail. The aim of this study was to create aluminum metal matrix composite castings based on aluminum alloys (AlSi11) reinforced with an Al<sub>2</sub>O<sub>3</sub> sinter preform using a Castability Trials spiral mold, and then to determine the degree of saturation with the liquid metal of the produced ceramic shaped body (Castability Trials spiral). For the selected AlSi11 alloy, the liquidus (Tl) and solidus (Ts) temperatures were determined by performing thermal-derivation analysis during cooling, which is Tl—579.3 °C and Ts—573.9 °C. The resultant pressure necessary for the infiltration process was estimated for the reinforcement capillaries with the following dimensions: 10, 15, 20, 25, 30 and 35 microns. The following values were used to determine the capillary pressure (Pk): surface tension of the alloy—σ = 840 mN/m; the extreme wetting angle of the reinforcement by the metal—θ = 136°. It has been experimentally confirmed that for the vacuum saturation process, the estimated resultant pressure enables saturation of reinforcement with capillaries larger than 25 microns, provided that the alloy temperature does not drop lower than the infiltration temperature. After the experiment, the time and route of the liquid metal flow in the spiral were determined. On the basis of the obtained values, a simulation was developed and initial assumptions such as saturation time, alloy temperature, reinforcement and mold temperature were verified. The energy balance showed that the saturation limit temperature was Tk = 580.7 °C for the reinforcement temperature of 575 °C. In contrast to the above, the assumption that the temperature of the metal after equalizing the temperature of the composite components must be higher than the liquidus temperature (Tliq = 579.3 °C) for the aluminum alloy used must be fulfilled. After the experiment, the time and path of the liquid metal flow in the spiral were determined. Then, on the basis of the obtained values, a simulation was developed, and the initial assumptions (saturation time and temperature) were verified.https://www.mdpi.com/1996-1944/16/18/6106castingaluminum metal matrix compositescastabilityenergy balance
spellingShingle Paweł Szymański
Paweł Popielarski
Dorota Czarnecka-Komorowska
Robert Sika
Katarzyna Gawdzińska
Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
Materials
casting
aluminum metal matrix composites
castability
energy balance
title Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
title_full Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
title_fullStr Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
title_full_unstemmed Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
title_short Determination of Saturation Conditions of the Aluminum Metal Matrix Composites Reinforced with Al<sub>2</sub>O<sub>3</sub> Sinter
title_sort determination of saturation conditions of the aluminum metal matrix composites reinforced with al sub 2 sub o sub 3 sub sinter
topic casting
aluminum metal matrix composites
castability
energy balance
url https://www.mdpi.com/1996-1944/16/18/6106
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AT dorotaczarneckakomorowska determinationofsaturationconditionsofthealuminummetalmatrixcompositesreinforcedwithalsub2subosub3subsinter
AT robertsika determinationofsaturationconditionsofthealuminummetalmatrixcompositesreinforcedwithalsub2subosub3subsinter
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