Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization

Core and layer polymer characterization of magnetite nanoparticles (NPs) surface-functionalized with poly(amidehydroxyurethane) (PAmHU), obtained by a new electrochemical synthesis route is presented. The core magnetic properties were investigated by Vibrating Sample Magnetometer (VSM), showing that...

Повний опис

Бібліографічні деталі
Автор: Laura Ursu
Формат: Стаття
Мова:English
Опубліковано: Publishing House of the Romanian Academy 2013-10-01
Серія:Memoirs of the Scientific Sections of the Romanian Academy
Предмети:
Онлайн доступ:http://mss.academiaromana-is.ro/mem_sc_st_2013/MSS%202013_1_Ursu.pdf
Опис
Резюме:Core and layer polymer characterization of magnetite nanoparticles (NPs) surface-functionalized with poly(amidehydroxyurethane) (PAmHU), obtained by a new electrochemical synthesis route is presented. The core magnetic properties were investigated by Vibrating Sample Magnetometer (VSM), showing that the obtained NPs have superparamagnetic to ferromagnetic behaviour (very low coercivity and remanence). The magnetite–PAmHU NPs morphology and size were studied by Atomic Force Microscopy (AFM) and Dynamic Light Scattering (DLS); both methods showed the existence of PAmHU out-flaked layer on NPs. Structural analysis by Infrared spectroscopy (FTIR) and Thermogravimetry (TG) confirm the out-flaking of magnetic NPs with PAmHU.
ISSN:1224-1407
2343-7049