Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization

Core and layer polymer characterization of magnetite nanoparticles (NPs) surface-functionalized with poly(amidehydroxyurethane) (PAmHU), obtained by a new electrochemical synthesis route is presented. The core magnetic properties were investigated by Vibrating Sample Magnetometer (VSM), showing that...

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প্রধান লেখক: Laura Ursu
বিন্যাস: প্রবন্ধ
ভাষা:English
প্রকাশিত: Publishing House of the Romanian Academy 2013-10-01
মালা:Memoirs of the Scientific Sections of the Romanian Academy
বিষয়গুলি:
অনলাইন ব্যবহার করুন:http://mss.academiaromana-is.ro/mem_sc_st_2013/MSS%202013_1_Ursu.pdf
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author Laura Ursu
author_facet Laura Ursu
author_sort Laura Ursu
collection DOAJ
description Core and layer polymer characterization of magnetite nanoparticles (NPs) surface-functionalized with poly(amidehydroxyurethane) (PAmHU), obtained by a new electrochemical synthesis route is presented. The core magnetic properties were investigated by Vibrating Sample Magnetometer (VSM), showing that the obtained NPs have superparamagnetic to ferromagnetic behaviour (very low coercivity and remanence). The magnetite–PAmHU NPs morphology and size were studied by Atomic Force Microscopy (AFM) and Dynamic Light Scattering (DLS); both methods showed the existence of PAmHU out-flaked layer on NPs. Structural analysis by Infrared spectroscopy (FTIR) and Thermogravimetry (TG) confirm the out-flaking of magnetic NPs with PAmHU.
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spelling doaj.art-b823f4d7d2ad4f4588b51d80b7055e342022-12-21T22:47:49ZengPublishing House of the Romanian AcademyMemoirs of the Scientific Sections of the Romanian Academy1224-14072343-70492013-10-01XXXVI71615Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterizationLaura Ursu0Advanced Research Center for Bionanoconjugates and Biopolymers, “Petru Poni” Institute of Macromolecular Chemistry, Iasi, RomaniaCore and layer polymer characterization of magnetite nanoparticles (NPs) surface-functionalized with poly(amidehydroxyurethane) (PAmHU), obtained by a new electrochemical synthesis route is presented. The core magnetic properties were investigated by Vibrating Sample Magnetometer (VSM), showing that the obtained NPs have superparamagnetic to ferromagnetic behaviour (very low coercivity and remanence). The magnetite–PAmHU NPs morphology and size were studied by Atomic Force Microscopy (AFM) and Dynamic Light Scattering (DLS); both methods showed the existence of PAmHU out-flaked layer on NPs. Structural analysis by Infrared spectroscopy (FTIR) and Thermogravimetry (TG) confirm the out-flaking of magnetic NPs with PAmHU.http://mss.academiaromana-is.ro/mem_sc_st_2013/MSS%202013_1_Ursu.pdfmagnetite–PAmHU capped NPscore and shell characterization
spellingShingle Laura Ursu
Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
Memoirs of the Scientific Sections of the Romanian Academy
magnetite–PAmHU capped NPs
core and shell characterization
title Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
title_full Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
title_fullStr Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
title_full_unstemmed Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
title_short Poly(amidehydroxyurethane) template magnetite NPs electrosynthesis. II. Core and shell characterization
title_sort poly amidehydroxyurethane template magnetite nps electrosynthesis ii core and shell characterization
topic magnetite–PAmHU capped NPs
core and shell characterization
url http://mss.academiaromana-is.ro/mem_sc_st_2013/MSS%202013_1_Ursu.pdf
work_keys_str_mv AT lauraursu polyamidehydroxyurethanetemplatemagnetitenpselectrosynthesisiicoreandshellcharacterization