The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ
The Sr doped La1Ba1-xSrx Ca2Cu4O8.5+δ samples with 0 ≤ x ≤ 0.3 had been prepared using the solid state reaction. The samples were claimed at 800°C for 3hr, palletized and sintered at 860°C for 20hr in air . Dielectric constant and loss by means of capacitance have been investigated wi...
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Format: | Article |
Language: | English |
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University of Baghdad
2017-04-01
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Series: | Ibn Al-Haitham Journal for Pure and Applied Sciences |
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Online Access: | https://jih.uobaghdad.edu.iq/index.php/j/article/view/375 |
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author | Kareem A. Jasim Mohammed A.N. Thejeel Raghad Subhi Al-Khafaji |
author_facet | Kareem A. Jasim Mohammed A.N. Thejeel Raghad Subhi Al-Khafaji |
author_sort | Kareem A. Jasim |
collection | DOAJ |
description |
The Sr doped La1Ba1-xSrx Ca2Cu4O8.5+δ samples with 0 ≤ x ≤ 0.3 had been prepared using the solid state reaction. The samples were claimed at 800°C for 3hr, palletized and sintered at 860°C for 20hr in air . Dielectric constant and loss by means of capacitance have been investigated with frequencies in the range of 1kHZ to 1MHZ for our samples at room temperature. Also, Shore hardness has been measured. The dielectric constant and loss decrease slightly with the increase of frequency for all compounds. Additionally, the partial substitution of Sr+2 into Ba+2 sites never have effect on the dielectric properties. X-ray diffraction (XRD) analysis showed a tetragonal structure and the as grown La1Ba1-xSrx Ca2Cu4O8.5+δ correspond to the 1124 phase. It was found that the change of the Sr concentrations of all our samples produces a change in a, c and c/a parameters.
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first_indexed | 2024-04-13T09:18:09Z |
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id | doaj.art-ba1a4838d773425aa639975f7573c8c7 |
institution | Directory Open Access Journal |
issn | 1609-4042 2521-3407 |
language | English |
last_indexed | 2024-04-13T09:18:09Z |
publishDate | 2017-04-01 |
publisher | University of Baghdad |
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series | Ibn Al-Haitham Journal for Pure and Applied Sciences |
spelling | doaj.art-ba1a4838d773425aa639975f7573c8c72022-12-22T02:52:41ZengUniversity of BaghdadIbn Al-Haitham Journal for Pure and Applied Sciences1609-40422521-34072017-04-01271The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δKareem A. JasimMohammed A.N. ThejeelRaghad Subhi Al-Khafaji The Sr doped La1Ba1-xSrx Ca2Cu4O8.5+δ samples with 0 ≤ x ≤ 0.3 had been prepared using the solid state reaction. The samples were claimed at 800°C for 3hr, palletized and sintered at 860°C for 20hr in air . Dielectric constant and loss by means of capacitance have been investigated with frequencies in the range of 1kHZ to 1MHZ for our samples at room temperature. Also, Shore hardness has been measured. The dielectric constant and loss decrease slightly with the increase of frequency for all compounds. Additionally, the partial substitution of Sr+2 into Ba+2 sites never have effect on the dielectric properties. X-ray diffraction (XRD) analysis showed a tetragonal structure and the as grown La1Ba1-xSrx Ca2Cu4O8.5+δ correspond to the 1124 phase. It was found that the change of the Sr concentrations of all our samples produces a change in a, c and c/a parameters. https://jih.uobaghdad.edu.iq/index.php/j/article/view/375La1Ba1-xSrx Ca2Cu4O8.5 δ, dielectric properties, Shore hardness |
spellingShingle | Kareem A. Jasim Mohammed A.N. Thejeel Raghad Subhi Al-Khafaji The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ Ibn Al-Haitham Journal for Pure and Applied Sciences La1Ba1-xSrx Ca2Cu4O8.5 δ, dielectric properties, Shore hardness |
title | The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ |
title_full | The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ |
title_fullStr | The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ |
title_full_unstemmed | The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ |
title_short | The Effect of Doping by Sr on the Structural, Mechanical and Electrical Characterization of La1Ba1-xSrx Ca2Cu4O8.5+δ |
title_sort | effect of doping by sr on the structural mechanical and electrical characterization of la1ba1 xsrx ca2cu4o8 5 i´ |
topic | La1Ba1-xSrx Ca2Cu4O8.5 δ, dielectric properties, Shore hardness |
url | https://jih.uobaghdad.edu.iq/index.php/j/article/view/375 |
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